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Record W2048079154 · doi:10.1002/cjce.20489

Preparation and characterisation of copper‐substituted SBA‐16 type mesoporous materials by modified pH‐adjusting method

2011· article· en· W2048079154 on OpenAlexvenueno aff
Asma Tufail Shah, Baoshan Li, Saeed Ahmad Nagra

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2011
Typearticle
Languageen
FieldMaterials Science
TopicMesoporous Materials and Catalysis
Canadian institutionsnot available
Fundersnot available
KeywordsChemistryNuclear chemistryMesoporous materialAqueous solutionCopperOrganic chemistryCatalysis

Abstract

fetched live from OpenAlex

Abstract Copper‐containing SBA‐16 type mesoporous material was synthesised by modified pH‐adjusting method at different pH values (pH 3, 5, and 7). In this method after formation of materials' basic structure the pH of mixture was adjusted with aqueous ammonia solution, stirred and filtered directly avoiding second hydrothermal treatment. The characterisation results revealed that copper was successfully incorporated into silica framework. The pH value was found to be a very important parameter in deciding the final structure, pH 5 was the most suitable pH value for preparation of ordered Cu‐SBA‐16, increase in pH to 7 resulted in formation of structure with less order. The material was applied for adsorption desulfurisation of dibenzothiophene (DBT) to check its performance.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.421

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.232
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations8
Published2011
Admission routes1
Has abstractyes

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