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Record W2049808629 · doi:10.1002/app.27958

Biocidal acyclic halamine polymers: Conversion of acrylamide‐<i>grafted</i>‐cotton to acyclic halamine

2008· article· en· W2049808629 on OpenAlexaff
Song Liu, Gang Sun

Bibliographic record

VenueJournal of Applied Polymer Science · 2008
Typearticle
Languageen
FieldChemistry
TopicAntimicrobial agents and applications
Canadian institutionsUniversity of Manitoba
Fundersnot available
KeywordsAmidePolymer chemistryPolymerPotassium persulfateYield (engineering)Fourier transform infrared spectroscopyCelluloseChemistryMaterials sciencePolymerizationOrganic chemistryChemical engineering

Abstract

fetched live from OpenAlex

Abstract Biocidal acyclic halamine materials can be prepared by chlorination of amide structures grafted onto polymers such as cellulose. This approach extended available halamine structures and potential applications in medical textiles and polymers. However, the conversion yield of the amide bonds to acyclic halamine was quite low (∼ 6%) according to the grafted amide bonds. By using instrumental analyses of FTIR, NMR, and LC‐MS, imidization reaction on amide bonds during the graft polymerization was identified as one of the major side reactions that could lead to the low conversion yield. Potassium persulfate was found accountable for the imidization reaction of amide structures. Potential solutions to this side reaction were proposed and evaluated as well in this study. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.007
Threshold uncertainty score0.935

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.235
Teacher spread0.223 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations25
Published2008
Admission routes1
Has abstractyes

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