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Record W2051914015 · doi:10.1021/jp003693e

Ab Initio Studies on the Mechanism of Tyrosine Coupling

2001· article· en· W2051914015 on OpenAlexaff
Igor L. Shamovsky, Richard J. Riopelle, Gregory M. Ross

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2001
Typearticle
Languageen
FieldChemistry
TopicFree Radicals and Antioxidants
Canadian institutionsQueen's University
Fundersnot available
KeywordsOxidative stressTyrosineChemistryDimerOxidative phosphorylationAb initioRadicalReactive oxygen speciesAmino acidBiophysicsBiochemistryOrganic chemistryBiology

Abstract

fetched live from OpenAlex

Oxidative stress is considered to be a major contributor to dysfunction in a host of disease states. Reactive oxygen species (ROS) mediate distinct oxidative alterations in biopolymers, including DNA, proteins, lipids, and lipoproteins. Currently, the mechanisms of biochemical reactions underlying oxidative stress are poorly understood because of the instability of ROS. One of the consequences of oxidative stress is one-electron oxidation of tyrosine (Tyr) residues in proteins, which represents a hallmark of this insult and is implicated in the pathogenesis of a number of pathological processes leading to atherosclerosis, inflammatory conditions, multiple system atrophy and several neurodegenerative diseases. Major products of oxidation of Tyr include protein-bound dityrosine and isodityrosine. In this report, the mechanism of tyrosine coupling (including structure and stability of a number of proposed reaction intermediates) is studied by high-level density functional and conventional ab initio methods including B3LYP, MP2, CASSCF, and CASPT2. It is demonstrated that dityrosine and isodityrosine are the most stable structures at all theoretical levels applied. In addition to classical structures of the reaction intermediates, evidence is found for a novel transient structure of Tyr dimer, stacked dityrosyl. This dimer is predicted to exist because of strong electron correlation between two tyrosyl moieties. The counterpoise corrected energy of stacked dityrosyl is below the energy of two tyrosyl radicals by about 95 kJ/mol at the PUMP2/6-31G** level. High proton affinity of tyrosyl radical (about 9.4 eV) suggests that positively charged amino acids in the vicinity of a solvent-exposed Tyr residue may increase the probability of tyrosine coupling.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.007
Threshold uncertainty score0.264

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.036
GPT teacher head0.281
Teacher spread0.245 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations39
Published2001
Admission routes1
Has abstractyes

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