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Record W2059872138 · doi:10.4212/cjhp.v64i4.1055

Stability of Ciprofloxacin in Polyvinylchloride Minibags

2011· article· en· W2059872138 on OpenAlexaffvenue
Ronald F Donnelly

Bibliographic record

VenueThe Canadian Journal of Hospital Pharmacy · 2011
Typearticle
Languageen
FieldMedicine
TopicAntibiotics Pharmacokinetics and Efficacy
Canadian institutionsCanadian Pharmacists Association
Fundersnot available
KeywordsCiprofloxacinDiluentChemistryChromatographyCiprofloxacin HydrochlorideHigh-performance liquid chromatographySodiumChemical stabilityNuclear chemistryAntibioticsOrganic chemistryBiochemistry

Abstract

fetched live from OpenAlex

Background: Ciprofloxacin is a fluoroquinolone antibiotic used to treat infections caused by both gram-positive and gram-negative organisms.Objective: To determine the physical and chemical stability of ciprofloxacin diluted in 5% dextrose in water (D5W) or 0.9% sodium chloride (normal saline [NS]) and stored in polyvinylchloride (PVC) minibags at various temperatures.Methods: Solutions of ciprofloxacin (1 and 2 mg/mL) were prepared by diluting a commercially available concentrate (10 mg/mL) with either D5W or NS. The prepared solutions were then packaged in PVC minibags. Three minibags of each concentration–diluent combination were stored at 2°C to 8°C with protection from light, at 21°C to 24°C with exposure to light, and at 29°C to 31°C with protection from light. Samples were collected from each minibag on days 0, 7, 14, and 30 and then analyzed. Colour, clarity, and pH were monitored when the samples were collected. On each day of analysis, the samples were accurately diluted before duplicate analysis with a stability-indicating high-performance liquid chromatography assay. A solution was considered stable if the concentration remained above 90% of the initial values.Results: There were no changes in the physical characteristics of any of the solutions. At both concentrations (1 and 2 mg/mL), the ciprofloxacin solutions prepared in D5W remained above 93.9% of the initial concentration over the 30-day study period under all 3 storage conditions. Similarly, at both concentrations, solutions diluted in NS remained above 95.9% of the initial concentration over the 30-day study period under all 3 storage conditions.Conclusions: Ciprofloxacin prepared in either D5W or NS and stored in PVC minibags was stable for 30 days under 3 separate storage conditions: 2°C to 8°C with protection from light, 21°C to 24°C with exposure to light, and 29°C to 31°C with protection from light.RÉSUMÉContexte : La ciprofloxacine est un antibiotique de la famille des fluoroquinolones utilisé dans le traitement des infections à bactéries Gram-positif et Gram-négatif.Objectif : Déterminer la stabilité physique et chimique de la ciprofloxacine diluée dans du dextrose à 5 % dans l’eau (D5E) ou dans du chlorure de sodium à 0,9 % (solution physiologique salée [SP]) conditionnée dans des minisacs de polychlorure de vinyle (PVC) entreposés à diverses températures.Méthodes : Les solutions de ciprofloxacine (concentrations de 1 et de 2 mg/mL) ont été préparées en diluant une préparation concentrée commercialisée (10 mg/mL) dans du D5E ou de la SP. Les solutions ainsi préparées ont été conditionnées dans des minisacs de PVC. Trois minisacs de chaque combinaison de concentration et de diluant ont été entreposés à une température de 2 °C à 8 °C, à l’abri de la lumière; de 21 °C à 24 °C, exposés à la lumière; et de 29 °C à 31 °C, à l’abri de la lumière. Des échantillons ont été prélevés de chaque minisac aux jours 0, 7, 14 et 30, puis analysés. La couleur, la limpidité et le pH ont été contrôlés lors du prélèvement des échantillons. Les jours d’analyse, les échantillons ont été dilués de façon précise avant qu’ils ne soient soumis à un double dosage au moyen d’une épreuve de stabilité par chromatographie liquide à haute pression. Une solution était jugée stable si la concentration se maintenait à plus de 90 % des valeurs initiales.Résultats : Aucun changement dans les caractéristiques physiques n’a été observé dans l’une ou l’autre des solutions. Pour les deux concentrations (1 et 2 mg/mL), les solutions de ciprofloxacine préparées dans du D5E ont conservé plus de 93,9 % de la concentration initiale pendant 30 jours dans les trois conditions d’entreposage. De même, pour les deux concentrations, les solutions diluées dans de la SP ont conservé plus de 95,9 % de la concentration initiale pendant 30 jours dans les trois conditions d’entreposage.Conclusions : Les solutions de ciprofloxacine préparées dans du D5E ou de la SP sont demeurées stables pendant 30 jours lorsqu’elles étaient conservées dans des minisacs de PVC à une température de 2 °C à 8 °C ou de 29 °C à 31 °C et à l’abri de la lumière, ou à une température de 21 °C à 24 °C, exposées à la lumière.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.056
GPT teacher head0.288
Teacher spread0.232 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations10
Published2011
Admission routes2
Has abstractyes

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