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Record W2061440912 · doi:10.1002/chem.200801606

Functional Mesoporous Material Derived from 3D Net‐Linked SBA‐15

2009· article· en· W2061440912 on OpenAlexaff
Yu Zhou, Ling Gao, Fangna Gu, Jia Yuan Yang, Jing Yang, Feng Wei, Ying Wang, Jian Zhu

Bibliographic record

VenueChemistry - A European Journal · 2009
Typearticle
Languageen
FieldMaterials Science
TopicMesoporous Materials and Catalysis
Canadian institutionsMinistry of Education and Child Care
FundersNational High-tech Research and Development ProgramNanjing UniversityGovernment of Jiangsu ProvinceNational Science Foundation
KeywordsMesoporous materialTetraethyl orthosilicatePorosityMaterials scienceOrthosilicateChemical engineeringMesoporous silicaAdsorptionAqueous solutionCubic zirconiaSmokeMorphology (biology)NanotechnologyChemistryCatalysisOrganic chemistryComposite materialCeramic

Abstract

fetched live from OpenAlex

A novel, versatile functional mesoporous material with the structure of SBA-15 but a specific 3D net-linked morphology has been prepared by using a facile method. This material has been assessed for its ability to reduce the level of nitrosamines in tobacco smoke so that the actual effect of this material in the reduction of carcinogenic environmental pollutants in a complex chemical system can be verified. By adjusting the force field during the hydrolysis and condensation processes of tetramethyl orthosilicate (TMOS) in an aqueous reaction system, the SBA-15 silica, which has a special morphology in that it is long and fiberlike from a microscopic view but large and block-like from a macroscopic angle, has been successfully synthesized. Moreover, the synthetic product is no longer a powder but a block because of its specific 3D net-linked morphology, which enables the material not only to trap particles in smoke but also to potentially be applied as a device. To strengthen the adsorptive capability of this porous material, a dry-impregnation procedure was applied in which zirconia was coated on the silica wall without changing the morphology. As expected, this functional material shows a high activity in the adsorption of N'-nitrosonornicotine (NNN), a bulky tobacco-specific nitrosamine, in solution and of N-nitrosopyrrolidine (NPYR), a volatile nitrosamine, in the gas stream. Furthermore, this 3D net-linked SBA-15 material can efficiently decrease the amount of nitrosamines and total number of particles in mainstream smoke when it is tested as an additive in the filter of a cigarette, thus providing powerful protection for the environment and public health.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesInsufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.041
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0420.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.204
Teacher spread0.190 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations27
Published2009
Admission routes1
Has abstractyes

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