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Diffusion of Hydrogen in Single Crystals of Monoclinic-ZrO<sub>2</sub> and Yttrium Stabilized Cubic Zirconia

2010· article· en· W2062841236 on OpenAlexfundno aff
D. Khatamian

Bibliographic record

VenueDefect and diffusion forum/Diffusion and defect data, solid state data. Part A, Defect and diffusion forum · 2010
Typearticle
Languageen
FieldMaterials Science
TopicNuclear Materials and Properties
Canadian institutionsnot available
FundersMcMaster University
KeywordsHydrogenMaterials scienceCubic zirconiaDiffusionOxideYttriumZirconiumThermal diffusivityMicrostructureSingle crystalAnalytical Chemistry (journal)CrystallographyChemistryThermodynamicsMetallurgyOrganic chemistry

Abstract

fetched live from OpenAlex

Transport of hydrogen through oxide layers formed on zirconium alloys has been the focus of studies associated with hydrogen ingress into nuclear reactor core components. The studies have shown that microstructure and microchemistry of the underlying alloy can affect the characteristics of the oxide and in turn the transport of hydrogen through the oxide and into the underlying metal. In certain cases the oxide layer can be a homogeneous medium for hydrogen diffusion, while in most cases it is found to be heterogeneous and comprised of homogeneous, nonporous and fully oxidized, cells surrounded by a network of fast diffusion paths for hydrogen. Since in such heterogeneous systems the derived diffusion parameter and the cell size are interdependent, an absolute diffusion parameter could only be derived if the cell size were known. However, no such information is available from the microstructural studies on the oxides grown on these alloys. Another alternative is to carry out the measurements in a material, which is homogeneous at least within the dimensions of a few μm - the range of the measurements. With this in mind, hydrogen diffusion measurements were carried out in a set of single crystal zirconia specimens with the prospect that the single crystals would provide a non-porous and homogeneous medium to study the diffusivity of hydrogen. These measurements show that the single crystal specimens, contrary to the initial thinking, are not entirely homogeneous and the results do not yield an absolute diffusion coefficient for hydrogen in zirconium oxides. The details and analyses of the results from the single crystal zirconia specimens are discussed in this paper.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.016

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.028
GPT teacher head0.269
Teacher spread0.241 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations16
Published2010
Admission routes1
Has abstractyes

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