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Production routes of the alpha emitting <sup>149</sup>Tb for medical application

2002· article· en· W2066902301 on OpenAlexfundno aff
G.J. Beyer, J. J. Čomor, Marko Daković, Dmitry Soloviev, C. Tamburella, E. Hagebø, Barbara J. Allan, S. N. Dmitriev, N.G. Zaitseva

Bibliographic record

VenueRadiochimica Acta · 2002
Typearticle
Languageen
FieldMedicine
TopicRadiopharmaceutical Chemistry and Applications
Canadian institutionsnot available
FundersTRIUMF
KeywordsSpallationChemistryAlpha particleRadiochemistryIonNuclear reactionIsotopeCyclotronYield (engineering)IrradiationAnalytical Chemistry (journal)Nuclear chemistryNuclear physicsPhysicsNeutron

Abstract

fetched live from OpenAlex

Summary The partial alpha emitting lanthanide isotope 149 Tb seems to have a great potential in systemic radioimmuno therapy (RIT), especially when single cells in transit or circulation are targeted. The isotope 149 Tb has a half life of 4.118 h and decays by alpha emission (3.97 MeV, 17%) EC-process (76%) and β + -emission (7%). In this paper, we analyze the possible production routes: light- and heavy ion induced nuclear reactions and p-induced spallation. The excitation functions for light- and heavy ion induced reactions have been calculated using the ALICE91 code. The direct nuclear reaction 152 Gd ( p , 4 n ) 149 Tb was found to be the most promising production path. Alternatively, the indirect reaction 142 Nd ( 12 C, 5 n ) 149 Dy → 149 Tb seems to be much more suitable compared to the reaction on the mono-isotopic target element 141 Pr 12 C, 4 n ) 149 Tb. In this case, both, the production yield of 149 Tb and the radionuclidic purity are considerably lower, compared to the ( p , 4 n )-reaction. In preliminary experiments we produced 149 Tb via the indirect reaction Nd ( 12 C, 5 n ) 149 Dy → 149 Tb (108 MeV 12 C +6 ions and 1 particle-µA) at the U-200 heavy ion cyclotron at the FLNR of the JINR Dubna. From a 1.25 h irradiation of a 12 mg/cm 2 nat Nd 2 O 3 target, we obtained 2.7 MBq of 149 Tb (70 µCi) at 20 min EOB. This allows the conclusion, that a dedicated cyclotron equipped with a modern ECR-ion source, providing high ion currents would allow the continuous production of batches of the order of 10–20 GBq of 149 Tb for routine RI-therapy. The lower cross section of the spallation process can be compensated by using very thick targets. On-line mass separation technique provides high purity isotopically clean 149 Tb preparations, independently on the production route chosen. At the ISOLDE facility at CERN, we prepared batches of up to 500 MBq 149 Tb by combining on-line mass separation process followed by a cation exchange chromatography process using α-HIBA as eluent. The obtained 149 Tb preparations showed excellent behavior in labeling of chelated monoclonal antibodies.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.156
Threshold uncertainty score0.405

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.023
GPT teacher head0.292
Teacher spread0.269 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations71
Published2002
Admission routes1
Has abstractyes

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