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Record W2067739406 · doi:10.2174/1874383800903010031

The Quest for a Fundamental Algorithm in X-Ray Fluorescence Analysis and Calibration

2009· article· en· W2067739406 on OpenAlexaff
Richard M. Rousseau

Bibliographic record

VenueThe Open Spectroscopy Journal · 2009
Typearticle
Languageen
FieldPhysics and Astronomy
TopicX-ray Spectroscopy and Fluorescence Analysis
Canadian institutionsGeological Survey of Canada
Fundersnot available
KeywordsCalibrationAlgorithmFlexibility (engineering)AnalyteSample (material)Intensity (physics)Matrix (chemical analysis)MathematicsComputer sciencePhysicsOpticsStatisticsChemistryThermodynamics

Abstract

fetched live from OpenAlex

The Fundamental Algorithm between concentration (C i ) and intensity (R i ) in X-ray fluorescence analysis is deduced from Sherman's equation without any approximation. Its explicit expression is thus theoretically exact and it corrects completely for all matrix effects on the intensity R i emitted by the analyte i in a given specimen. This powerful algorithm combines the practical flexibility of the influence coefficient concept and the theoretical exactness of the Fundamental-Parameters method. In association with its innovative calibration procedure, the Fundamental Algorithm can be applied to the analysis of any sample type and offers maximum accuracy, limited only by the quality of sample preparation and the standards used.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.013
metaresearch head score (Gemma)0.029
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Methods · Consensus signal: Methods
Teacher disagreement score0.013
Threshold uncertainty score0.068

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0130.029
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0020.002
Science and technology studies0.0010.008
Scholarly communication0.0050.010
Open science0.0040.004
Research integrity0.0030.007
Insufficient payload (model declined to judge)0.0020.004

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.300
Teacher spread0.292 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreMethods

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations40
Published2009
Admission routes1
Has abstractyes

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