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Record W2067793891 · doi:10.1107/s0108767305088653

Macromolecular crystallography at room temperature: wavelength dependence radiation sensitivity and damage

2005· article· en· W2067793891 on OpenAlexaff
Mehmet Aslantaş, Engin Kendi, V. Stojanoff

Bibliographic record

VenueActa Crystallographica Section A Foundations of Crystallography · 2005
Typearticle
Languageen
FieldMaterials Science
TopicEnzyme Structure and Function
Canadian institutionsInstitute of Infection and Immunity
Fundersnot available
KeywordsWavelengthSensitivity (control systems)Radiation damageMaterials scienceCrystallographyRadiation sensitivityRadiationMacromoleculeChemistryOptoelectronicsIrradiationOpticsPhysicsBiochemistryNuclear physicsEngineering

Abstract

fetched live from OpenAlex

Streptococcal organisms share a well-conserved, binding protein dependent, Multiple Sugar Metabolism (msm) system which is responsible for the transportation and metabolism of multiple sugars.This system is comprised of 8 proteins including 2 membrane proteins (MsmF and MsmG), an ATP-binding protein (MsmK) and the 45KDa sugar-binding lipoprotein MsmE [1].Both native and selenomethionine derivatised MsmE were crystallised in space group P6 1 22.Selenomethionine derivative crystals showed diffraction to 2.5Å and 3-wavelength MAD data were collected at SRS, Daresbury.Selenium sites (19/22) were found using SnB [2] with peak data and site refinement and phasing using Sharp/AutoSharp [3] using MAD data along with a 3Å native dataset.The initial model shows a two domain periplasmic binding protein-like fold and model-building and refinement is continuing.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.020

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.002
Science and technology studies0.0010.000
Scholarly communication0.0010.001
Open science0.0010.000
Research integrity0.0000.002
Insufficient payload (model declined to judge)0.0060.002

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.220
Teacher spread0.214 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2005
Admission routes1
Has abstractyes

Explore more

Same venueActa Crystallographica Section A Foundations of CrystallographySame topicEnzyme Structure and FunctionFrench-language works237,207