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Record W2069578235 · doi:10.1021/jp0309264

Thiophosgene, A Molecule Tailor-Made for Testing Fundamental Theoretical Concepts of Radiationless Transitions:  Intramolecular Dynamics of S<sub>1</sub>Cl<sub>2</sub>CS

2003· article· en· W2069578235 on OpenAlexaff
Takashige Fujiwara, D. C. Moule, Edward C. Lim

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2003
Typearticle
Languageen
FieldChemistry
TopicOrganic Chemistry Cycloaddition Reactions
Canadian institutionsBrock University
Fundersnot available
KeywordsIntramolecular forceMoleculeDynamics (music)Computational chemistryChemistryChemical physicsNanotechnologyMaterials sciencePhysicsStereochemistryOrganic chemistry

Abstract

fetched live from OpenAlex

The collision-free S 1 [à 1 A 2 (nπ*)] thiophosgene, with small (<3484 cm -1 ) and large (>9284 cm -1 ) excess vibrational energies, does not exhibit radiationless transitions to bound electronic states (S 0 and T 1 ), as evidenced by intense à → X̃ fluorescence with nearly constant lifetimes. The lack of radiationless transitions can be traced to the absence of the promoting mode for the 1 A 2 → 1 A 1 internal conversion and the vanishingly small spin−orbit coupling and very small Franck−Condon factor for the 1 A 2 (nπ*) → 3 A 2 (nπ*) intersystem crossing. In the intermediate range of excess energies (3484−9284 cm -1 ), fluorescence is not observed, consistent with the occurrence of predissociation. Quantum beat-modulated fluorescence decays, attributable to 1 A 2 (nπ*)− 3 A 1 (ππ*) perturbations, have been observed for excitation of 1 1 2 1 3 1 4 1 and nearby S 1 vibronic levels. This places the b̃ 3 A 1 (ππ*) state at about 20 350 cm -1 above the ground electronic state, in excellent agreement with the existing estimate. Interestingly, the S 1 radiative lifetime is about an order of magnitude shorter in a supersonic jet as compared to the vapor phase at room temperature, indicating that the probability of the vibronically induced à 1 A 2 (nπ*)−X̃ 1 A 1 radiative transition is significantly reduced at higher temperatures, due probably to Coriolis coupling.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Theoretical or conceptual · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.233
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designTheoretical or conceptual
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations15
Published2003
Admission routes1
Has abstractyes

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Same venueThe Journal of Physical Chemistry ASame topicOrganic Chemistry Cycloaddition ReactionsFrench-language works237,207