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Study on Phase Diagram of Ca<sub>3</sub>NbGa<sub>3</sub>Si<sub>2</sub>O<sub>14</sub> Piezoelectric Material by Differential Thermal Analysis and X-Ray Diffraction Measurement

2012· article· en· W2075049888 on OpenAlex
Yoshisuke Futami, Yuui Yokota, Masato Sato, Kazushige Tota, Jan Pejchal, Takayuki Yanagida, Ko Onodera, Akira Yoshikawa

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueKey engineering materials · 2012
Typearticle
Languageen
FieldEngineering
TopicAcoustic Wave Resonator Technologies
Canadian institutionsHatch (Canada)
Fundersnot available
KeywordsImpurityStoichiometryMelting pointPhase diagramAnalytical Chemistry (journal)Materials sciencePhase (matter)Melting temperatureCrystal (programming language)Solid solutionCongruent meltingCrystallographyChemistryPhysical chemistryMetallurgy

Abstract

fetched live from OpenAlex

Ca 3 NbGa 3 Si 2 O 14 (CNGS) Is One of the Langasite-Type Crystals and it Is Known as a Piezoelectric Material. We Have Successfully Grown the Shaped CNGS Crystal Using Micro-Pulling-down (μ-PD) Method with Shape Control. However, the Impurity Phases such as Ca-Nb-O Related Compounds Were Detected in the Grown Crystals. The Creation of the Impurity Phases Is Related to Difference in Stoichiometric and Congruent Compositions. Therefore, the Detailed Investigation of Phase Diagram on CNGS Was Carried Out to Prevent the Impurity Phases Creation. It Follows from the TG-DTA Measurements that the Melting Point Systematically Changed with the Ca/Ga Ratio in the Ca 3-x NbGa 3+x Si 2 O 14±δ Cmpositions. The CNGS Phase with Ca/Ga = 1.02 Indicated the Maximum Melting Point which Suggests that the Stoichiometric Composition of CNGS Is Different in the Congruent Composition. Furthermore, in the DTA Measurements the Peaks of Impurity Phases Were Detected around 1550 °C for the CNGS Sample with Ca/Ga = 1.02.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.005
metaresearch head score (Gemma)0.002
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Scholarly communication, Research integrity
Consensus categoriesMeta-epidemiology (narrow), Research integrity
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.033
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0050.002
Meta-epidemiology (narrow)0.0060.007
Meta-epidemiology (broad)0.0080.002
Bibliometrics0.0050.005
Science and technology studies0.0010.001
Scholarly communication0.0020.002
Open science0.0040.002
Research integrity0.0040.003
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.215
Teacher spread0.204 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it