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Record W2079559214 · doi:10.1179/cmq.2008.47.3.269

ONLINE FREE ACIDITY MEASUREMENT OF SOLUTIONS CONTAINING BASE METALS

2008· article· en· W2079559214 on OpenAlexfundno aff
Ming Huang, Vladimiros G. Papangelakis

Bibliographic record

VenueCanadian Metallurgical Quarterly · 2008
Typearticle
Languageen
FieldChemical Engineering
TopicChemical and Physical Properties in Aqueous Solutions
Canadian institutionsnot available
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsConductivityChlorideBase (topology)ElectrolyteAnalytical Chemistry (journal)ChemistrySulfateMetalMineralogyInorganic chemistryEnvironmental chemistryMaterials scienceMetallurgyPhysical chemistryMathematicsElectrode

Abstract

fetched live from OpenAlex

AbstractElectrodeless conductivity was employed to investigate the feasibility of continuous online monitoring of the free acidity of sulphate and/or chloride solutions of Cu and other base metals from various hydrometallurgical processes. These solutions were measured with both commercial and experimental electrodeless conductivity sensors from 15 to 250 °C. It was confirmed that hydrogen ion has the greatest impact on conductivity by carrying the bulk of the current because it is the most mobile ion. In combination with a solution speciation analysis the conductivity sensor can be calibrated to account for the contribution of Cu electrolytes as well as other dissolved salts allowing fast and accurate online measurement of free acid. The sensor was tested at both lab and pilot scale with very good performance. The average difference between the measured and the titrated acid concentration was less than 5%, which is excellent for industrial applications.On a employé la conductivité sans électrodes pour investiguer la faisabilité de surveillance continue en ligne de l’acidité libre de solutions de sulfate et/ou de chlorure de Cu et d’autres métaux de base de divers procédés d’hydrométallurgie. On a mesuré ces solutions avec des capteurs de conductivité sans électrodes tant commerciaux qu’expérimentaux dans la gamme de 15 à 250 °C. On a confirmé que l’ion hydrogène avait le plus grand impact sur la conductivité en transportant la majorité du courant parce que c’est l’ion le plus mobile. En combinaison avec une analyse de spéciation de solution, on peut calibrer le capteur de conductivité pour tenir compte de la contribution des électrolytes de Cu ainsi que d’autres sels dissous, permettant la mesure en ligne rapide et précise de l’acide libre. On a évalué le capteur tant au laboratoire qu’à l’échelle pilote avec un très bon rendement. La différence moyenne entre la concentration d’acide mesurée et titrée était de moins que 5%, ce qui est excellent pour les applications industrielles.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.770
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.068
GPT teacher head0.225
Teacher spread0.157 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2008
Admission routes1
Has abstractyes

Explore more

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