Facile synthesis of exfoliated and highly conductive poly(arylene disulfide)/graphite nanocomposites
Why this work is in the frame
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Bibliographic record
Abstract
Abstract Exfoliated graphite has been synthesized by first synthesizing H 2 SO 4 intercalated compound in a H 2 O 2 ‐H 2 SO 4 mixture, followed by exfoliation under microwave irradiation. Poly(arylene disulfide)/graphite nanocomposites were then fabricated by absorbing cyclic(arylene disulfide) oligomers into the pores of exfoliated graphite. Subsequently, the nanocomposite precursor was subjected to heat treatment to carry out the in situ ring‐opening polymerization of the oligomers via free radical mechanism. The as‐prepared nanocomposite exhibited a exfoliated nanostructure as evidenced by transmission electron microscopy (TEM) observation. The nanocomposite with a very small amount of graphite, 5 wt%, possesses a highly electrical conductivity of 4 S/cm, therefore, many applications can be found as conductive materials. Copyright © 2004 John Wiley & Sons, Ltd.
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Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.001 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.000 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it