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Record W2086512751 · doi:10.1021/jp0025227

Stark Spectroscopic Studies of Blue Copper Proteins:  Azurin

2000· article· en· W2086512751 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueThe Journal of Physical Chemistry B · 2000
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicProtein Interaction Studies and Fluorescence Analysis
Canadian institutionsUniversity of Alberta
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsAzurinCopper proteinGround stateCopperPolarizabilityChemistryDipoleContext (archaeology)Excited stateAtomic physicsMolecular physicsCrystallographyChemical physicsPhysicsMoleculeOrganic chemistry

Abstract

fetched live from OpenAlex

The change in the dipole moments (| |) and the average change in the polarizability (〈 Δα 〉) upon excitation for the Cys(S)⇒Cu(II) ligand-to-metal charge-transfer (LMCT) transitions in two species of azurin, a type I blue copper protein from A lcaligenes denitrificans (AD) and Pseudomonas aeruginosa (PA), were determined using Stark (electroabsorption) spectroscopy. Measurements at 77 K in a glycerol-water glassy matrix yield a value for | | of between 1.3 and 2.0 D. This value of | | is consistent with the highly covalent nature of the S Cu bond in the ground state and is in agreement with the predictions of previous electronic structure calculations. The polarizability of the excited state was smaller than the ground state by about 10−20 Å 3 . This negative value of 〈 Δα 〉, which is somewhat unusual, is interpreted in the context of the two-state model. Values for the electron-transfer matrix element ( H ab ) and the effective charge-transfer distance ( R ab ) derived from our measurements are also reported.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.280

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.293
Teacher spread0.281 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it