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Record W2086675143 · doi:10.1180/minmag.2011.075.2.303

Holtite and dumortierite from the Szklary Pegmatite, Lower Silesia, Poland

2011· article· en· W2086675143 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMineralogical Magazine · 2011
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsUniversity of British Columbia
FundersUniwersytet WarszawskiUniversity of British Columbia
KeywordsPegmatiteBearing (navigation)HomogeneousMineralCrystallizationCrystallographyGeologyMineralogyMaterials scienceMetallurgyChemistry

Abstract

fetched live from OpenAlex

Abstract The Szklary holtite is represented by three compositional varieties: (1) Ta-bearing (up to 14.66 wt.% Ta 2 O 5 ), which forms homogeneous crystals and cores within zoned crystals; (2) Ti-bearing (up to 3.82 wt.% TiO 2 ), found as small domains within the core; and (3) Nb-bearing (up to 5.30 wt.% Nb 2 O 5 ,) forming the rims of zoned crystals. All three varieties show variable Sb+As content, reaching 19.18 wt.% Sb 2 O 3 (0.87 Sb a.p.f.u.) and 3.30 wt.% As 2 O 3 (0.22 As a.p.f.u.) in zoned Ta-bearing holtite, which constitutes the largest Sb+As content reported for the mineral. The zoning in holtite is a result of Ta-Nb fractionation in the parental pegmatite-forming melt together with contamination of the relatively thin Szklary dyke by Fe, Mg and Ti. Holtite and the As- and Sb-bearing dumortierite, which in places overgrows the youngest Nb-bearing zone, suggest the following crystallization sequence: Ta-bearing holtite → Ti-bearing holtite → Nb-bearing holtite → As- and Sb-bearing, (Ta,Nb,Ti)-poor dumortierite → As- and Sb-dominant, (Ta,Nb,Ti)-free dumortierite-like mineral (16.81 wt.% As 2 O 3 and 10.23 wt.% Sb 2 O 3 ) with (As+Sb) > Si. The last phase is potentially a new mineral species. Al 6 □☐(Sb,As) 3 O 15 , or Al 5 ☐ 2 B(Sb,As) 3 O 12 (OH) 3 , belonging to the dumortierite group. The Szklary holtite shows no evidence of clustering of compositions around ‘holtite I’ and ‘holtite II'. Instead, the substitutions of Si 4+ by Sb 3+ +As 3+ at the Si/Sb sites and of Ta 5+ by Nb 5+ or Ti 4+ at the Al(l) site suggest possible solid solutions between: (1) (Sb,As)-poor and (Sb,As)-rich holtite; (2) dumortierite and the unnamed (As+Sb)-dominant dumortierite-like mineral; and (3) Ti-bearing dumortierite and holtite. i.e. our data provide further evidence for miscibility between holtite and dumortierite, but leave open the question of defining the distinction between them. The Szklary holtite crystallized from the melt along with other primary Ta-Nb-(Ti) minerals such as columbite-(Mn), tantalite-(Mn), stibiotantalite and stibiocolumbite as the availability of Ta decreased. The origin of the parental melt can be related to anatexis in the adjacent Sowie Mountains complex, leading to widespread migmatization and metamorphic segregation in pelitic-psammitic sediments metamorphosed at ∼390—380 Ma.

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Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.982
Threshold uncertainty score0.995

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0060.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.028
GPT teacher head0.199
Teacher spread0.171 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it