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Record W2101962900 · doi:10.1149/1.3328506

Active Site and Electrocatalytic Behavior at Palladium Electrode Surfaces

2010· article· en· W2101962900 on OpenAlex
Lorraine C. Nagle, Sébastien Garbarino, Declan Burke

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueECS Transactions · 2010
Typearticle
Languageen
FieldEnergy
TopicElectrocatalysts for Energy Conversion
Canadian institutionsInstitut National de la Recherche Scientifique
Fundersnot available
KeywordsPalladiumFormic acidCatalysisChemistryInorganic chemistryRedoxElectrodeElectrocatalystPhotochemistryElectrochemistryOrganic chemistryPhysical chemistry

Abstract

fetched live from OpenAlex

The electrocatalytic properties of palladium are of interest in connection with direct formic acid fuel cell development. Cyclic voltammograms recorded for activated palladium electrodes in sulphuric acid solution exhibit a quasi-reversible surface redox transition at ca. 0.25 V (RHE) and, in the presence of formic acid, the oxidation of the latter undergoes a dramatic change in rate at the same potential. Catalysis in this case evidently involves surface active site behaviour, low coverage protruding palladium species undergoing oxidation in a repetitive manner, the resulting surface cations coordinating bisulphate anions and acting as mediators for the formic acid oxidation reaction.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.037
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0010.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.212
Teacher spread0.207 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it