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Record W2102064591 · doi:10.1002/masy.200900015

Synthesis of Polyacrylic/Silica Nanocomposite Latexes using Static Mixer

2010· article· en· W2102064591 on OpenAlexaff
Gholamali Farzi, Élodie Bourgeat‐Lami, Timothy F. L. McKenna

Bibliographic record

VenueMacromolecular Symposia · 2010
Typearticle
Languageen
FieldChemistry
TopicAdvanced Polymer Synthesis and Characterization
Canadian institutionsQueen's University
Fundersnot available
KeywordsMaterials scienceNanocompositeNucleationPolymerizationChemical engineeringMiniemulsionHydrophobic silicaHomogeneousDispersityViscosityPolymerEmulsion polymerizationPolymer chemistryComposite materialChemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Summary: Static mixers (Sulzer Chemtech; SMX) were used to prepare silica/ MMA‐co‐BA miniemulsions that were polymerized to produce nanocomposite latexes. Acceptable conditions for the formulation of polymerizable nanodroplets were found and subsequently used to produce silica/poly(MMA‐co‐BA) nanocomposites. The droplet size distribution of the resulting miniemulsions was narrow enough that it could be successfully polymerized. It was found that the droplet size depends on the silica content and increases with increasing the silica concentration. It was also shown that there is a relationship between the droplet size and the viscosity of the dispersed phase. The majority of droplets were nucleated upon polymerization when less than 15% silica was used. However, when the silica content exceeded 15%, the ratio of the number of particles in the final latex to the number of droplets (Np/Nd) increased to value much higher than 1 indicating the occurrence of homogeneous nucleation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.227
Teacher spread0.222 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations7
Published2010
Admission routes1
Has abstractyes

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