Electrocatalytic oxidation of hydrazine by copper iodide modified sol-gel derived carbon-ceramic composite Electrode
Bibliographic record
Abstract
A new sol-gel derived ceramic-carbon composite electrode was fabricated by the use of CuI as modifier.The electrocatalytic activity of the copper iodide modified sol-gel derived ceramiccarbon composite (CIM-SGD-CCC) electrode was examined for the oxidation of hydrazine.Cyclic voltammetry was employed to study the electrochemical and electrocatalytic properties of the modified electrode.Results showed that the CIM-SGD-CCC electrode has very high catalytic activity for electrooxidation of hydrazine.This proves that the copper iodide bears the main role in electro-catalytic oxidation of hydrazine.This modified electrode shows fast amperometric response with the range from 1 μ mol L -1 to 40 μ mol L -1 and the limit of detection (LOD) of 0.524 μ mol L -1 for hydrazine.The relative standard deviation (R.S.D.) was 0.72 % for 5 successive assays.High stability, good reproducibility, rapid response, easy surface regeneration and fabrication are the important characteristics of the proposed electrode.
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How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.001 | 0.000 |
| Meta-epidemiology (broad) | 0.001 | 0.001 |
| Bibliometrics | 0.001 | 0.001 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.001 | 0.000 |
| Research integrity | 0.001 | 0.001 |
| Insufficient payload (model declined to judge) | 0.001 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".