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Record W2108210110 · doi:10.1180/minmag.2008.072.3.747

Mushroom elbaite from the Kat Chay mine, Momeik, near Mogok, Myanmar: I. Crystal chemistry by SREF, EMPA, MAS NMR and Mössbauer spectroscopy

2008· article· en· W2108210110 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMineralogical Magazine · 2008
Typearticle
Languageen
FieldEarth and Planetary Sciences
TopicMineralogy and Gemology Studies
Canadian institutionsUniversity of Manitoba
FundersNatural Sciences and Engineering Research Council of CanadaCanada Research ChairsUniversity of Manitoba
KeywordsEMPAMössbauer spectroscopyTourmalineChemistrySpectroscopyAnalytical Chemistry (journal)ParamagnetismCrystallographyMagic angle spinningElectron microprobeMineralogyNuclear magnetic resonance spectroscopyMaterials sciencePhysicsCondensed matter physicsStereochemistryMetallurgy

Abstract

fetched live from OpenAlex

Abstract Tourmaline from the Kat Chay mine, Momeik, near Mogok, Shan state, Myanmar, shows a variety of habits that resemble mushrooms, and it is commonly referred to as ‘mushroom tourmaline'. The structure of nine single crystals of elbaite, ranging in colour from pink to white to black and purple, extracted from two samples of mushroom tourmaline from Mogok, have been refined (SREF) to R indices of ~2.5% using graphite-monochromated Mo- K α X-radiation. 11 B and 27 Al Magic Angle Spinning Nuclear Magnetic Resonance spectroscopy shows the presence of [4] B and the absence of [4] Al in samples with transition-metal content low enough to prevent paramagnetic quenching of the signal. Site populations were assigned from refined site-scattering values and unit formulae derived from electron-microprobe analyses of the crystals used for X-ray data collection. 57 Fe Mössbauer spectroscopy shows that both Fe 2+ and Fe 3+ are present, and the site populations derived by structure refinement show that there is no Fe at the Z site; hence all Fe 2+ and Fe 3+ occurs at the Y site. The 57 Fe Mössbauer spectra also show peaks due to intervalence charge-transfer involving Fe 2+ and Fe 3+ at adjacent Y sites. Calculation of the probability of the total amount of Fe occurring as Fe 2+ –Fe 3+ pairs for a random short-range distribution is in close accord with the observed amount of Fe involved in Fe 2+ –Fe 3+ , indicating that there is no short-range order involving Fe 2+ and Fe 3+ in these tourmalines.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: Observational
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.313
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0010.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0070.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.196
Teacher spread0.183 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it