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Biomolecular <scp>NMR</scp> Spectroscopy of Ribonucleic Acids

2014· other· en· W2112500913 on OpenAlexaff
Thorsten Dieckmann, Michael Piazza, Éric Bonneau, Pascale Legault

Bibliographic record

VenueEncyclopedia of Life Sciences · 2014
Typeother
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicRNA and protein synthesis mechanisms
Canadian institutionsUniversité de MontréalUniversity of Waterloo
Fundersnot available
KeywordsNuclear magnetic resonance spectroscopyChemistryNuclear magnetic resonance spectroscopy of nucleic acidsRNARibozymeFluorine-19 NMRNucleic acidNucleobaseNucleic acid structureRiboswitchSmall moleculeNucleotideMoleculeSpectroscopyAptamerTwo-dimensional nuclear magnetic resonance spectroscopyIntramolecular forceTransverse relaxation-optimized spectroscopyStereochemistryBiochemistryNon-coding RNADNAOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Biomolecular nuclear magnetic resonance (NMR) spectroscopy allows the characterisation of structural and dynamic properties of ribonucleic acids (RNAs) in solution. The NMR‐based determination of high‐resolution three‐dimensional (3D) structures by NMR spectroscopy in solution is especially useful for small‐to‐medium sized RNA molecules like aptamers and small ribozymes, but has also been achieved for RNAs up to about 100 nucleotides in total size. Biomolecular NMR also provides valuable information about the interaction between RNA and diverse binding partners such as drugs, peptides, proteins or other nucleic acids. In addition, novel methods can be utilised to characterise the role of metal ions, intramolecular dynamics across a range of motion time scales and shifted p K a values of exchangeable nucleobase protons in RNA structure and catalysis. Key Concepts: High‐resolution NMR spectroscopy in solution is a powerful method to determine the 3D structures of small and medium sized RNA molecule. The structure determination of larger RNAs generally requires labelling with stable isotopes The information about molecular dynamics that can be obtained by NMR experiments allows quantitative studies of molecular motion across a wide range of time scales. The possibility to directly observe changes in the pK a values of ionisable groups. The localisation of divalent metal ions can be defined using several NMR methods.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Other · Consensus signal: Other
Teacher disagreement score0.421
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.245
Teacher spread0.237 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2014
Admission routes1
Has abstractyes

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