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High‐Temperature Neutron Diffraction of the AlN–Al <sub>2</sub> O <sub>3</sub> –Y <sub>2</sub> O <sub>3</sub> System

2003· article· en· W2123271635 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of the American Ceramic Society · 2003
Typearticle
Languageen
FieldMaterials Science
TopicAdvanced ceramic materials synthesis
Canadian institutionsMcGill UniversityRoyal Military College of CanadaNational Research Council CanadaConcordia University
Fundersnot available
KeywordsMaterials sciencePhase diagramTernary operationNitrideAtmospheric temperature rangeTernary numeral systemPhase (matter)Analytical Chemistry (journal)ThermodynamicsNeutron diffractionCrystallographyComposite materialCrystal structureChemistry

Abstract

fetched live from OpenAlex

The importance of aluminum nitride (AlN) stems from its application in microelectronics as a substrate material due to high thermal conductivity, high electrical resistance, mechanical strength and hardness, thermal durability, and chemical stability. Yttria (Y 2 O 3 ) is the best additive for AlN sintering. AlN densifies by a liquid‐phase mechanism, where the surface oxide, Al 2 O 3 , reacts with Y 2 O 3 to form an Y‐Al‐O‐N liquid that promotes particle rearrangement and densification. Construction of the phase relations in this multicomponent system is essential for optimizing the properties of AlN. The ternary phase diagram of the AlN–Al 2 O 3 –Y 2 O 3 was developed by Gibbs energy minimization using interpolation procedures based on modeling the binary subsystems. This paper aims at testing the resultant understanding experimentally at selected compositions using in situ high‐temperature neutron diffractometry. These experimental results agree with the thermodynamic calculations of AlN–Al 2 O 3 –Y 2 O 3 . The ternary phase diagram has been constructed for the first time in this work. High‐temperature neutron diffractometry has permitted real time measurement of the reactions involved in this ternary system, especially to determine the temperature range for each reaction, which would have been difficult to establish by other means.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies
Consensus categoriesMeta-epidemiology (narrow)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.012
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0030.001
Meta-epidemiology (narrow)0.0020.001
Meta-epidemiology (broad)0.0030.002
Bibliometrics0.0000.002
Science and technology studies0.0010.002
Scholarly communication0.0010.001
Open science0.0030.001
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.213
Teacher spread0.207 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it