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Record W2123304747 · doi:10.1177/0040517511407376

Thermal characteristics and physical properties of silk fabrics grafted with phosphorous flame retardant agents

2011· article· en· W2123304747 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueTextile Research Journal · 2011
Typearticle
Languageen
FieldMaterials Science
TopicSilk-based biomaterials and applications
Canadian institutionsUniversity of Manitoba
Fundersnot available
KeywordsFire retardantMaterials scienceSILKCopolymerThermogravimetric analysisFibroinThermal decompositionThermal stabilityComposite materialGraftingUltimate tensile strengthMonomerPolymer chemistryChemical engineeringPolymerChemistryOrganic chemistry

Abstract

fetched live from OpenAlex

The production of flame retardant silk fabrics is very challenging and there is limited technology available on fire retardant silk applications. In this study, two flame retardant monomers having phosphoric groups, phosmer M and phosmer CL, were applied onto silk fabrics by a graft copolymerization technique. The grafted silk fabrics showed a high level of flame retardancy as evaluated by Japanese Industrial Standard micro-burner test method. It was shown that grafting techniques using phosmer CL are more effective than those using phosmer M to enhance the flame retardant functional properties of the silk fabrics. The differential scanning calorimetry, thermogravimetric analysis and thermomechanical analysis showed that the thermal stability of silk fibroin molecules was greatly enhanced by graft copolymerization with the used phosmers. The position of thermal decomposition for silk fabric shifted toward higher temperature after graft copolymerization with phosmer CL and M. Fourier transform infrared spectra showed evidence of the reaction between the used phosmers and silk. However, the surface morphology of silk fiber was very smooth and fine, and the tensile strength was not significantly affected regardless of the graft copolymerization with phosmer M and CL.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.031
Threshold uncertainty score0.443

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.094
GPT teacher head0.311
Teacher spread0.217 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it