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Record W2125237562 · doi:10.1139/v11-062

<sup>129</sup>Xe and <sup>2</sup>H nuclear magnetic resonance (NMR) of xenon and deuterated-chloroform solutes in a thermotropic biaxial nematic liquid crystal

2011· article· en· W2125237562 on OpenAlexvenueno aff
Pekka Tallavaara, Anu M. Kantola, Jukka Jokisaari, T. Meyer, Daniela A. Wilson, Georg H. Mehl

Bibliographic record

VenueCanadian Journal of Chemistry · 2011
Typearticle
Languageen
FieldMaterials Science
TopicLiquid Crystal Research Advancements
Canadian institutionsnot available
Fundersnot available
KeywordsThermotropic crystalLiquid crystalChemistryXenonDeuterium NMRNuclear magnetic resonance spectroscopyPhase (matter)ChloroformDeuteriumNuclear magnetic resonanceAnalytical Chemistry (journal)MoleculeMaterials scienceStereochemistryOrganic chemistryAtomic physicsLiquid crystalline

Abstract

fetched live from OpenAlex

Properties of a thermotropic nematic liquid crystal (LC) TM35 (organosiloxane tetrapode) were investigated by means of nuclear magnetic resonance (NMR) spectroscopy of probe atoms and molecules. 129 Xe isotope enriched xenon gas and 2 H isotope enriched chloroform were used as probes. Both 129 Xe and 2 H NMR measurements were carried out over a wide temperature range, covering isotropic, nematic, and glass phases. A clear change in the behavior of the LC is observed within the nematic phase at 289 K by changing the temperature from low to high and inspecting the spectral line width. The derivative curve of the 129 Xe chemical shift also reveals a change at 289 K. These changes may be an indication of hindered molecular rotation around the long axis, and the appearance of a biaxial nematic phase.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.063
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.218
Teacher spread0.203 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2011
Admission routes1
Has abstractyes

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