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Microstructural Parameters of HPMC/PVP Polymer Blends Using Wide Angle X-Ray Technique

2012· article· en· W2134516701 on OpenAlexvenueno aff
Y. Prakash, H. Somashekarappa, T. Demappa, R. Somashekar

Bibliographic record

VenueJournal of Research Updates in Polymer Science · 2012
Typearticle
Languageen
FieldMaterials Science
TopicPolymer Nanocomposite Synthesis and Irradiation
Canadian institutionsnot available
Fundersnot available
KeywordsMaterials sciencePolyvinylpyrrolidoneCrystallitePolymerScanning electron microscopeUltimate tensile strengthComposite materialPolymer blendWide-angle X-ray scatteringScatteringSmall-angle neutron scatteringPolymer chemistryOpticsNeutron scatteringCopolymer

Abstract

fetched live from OpenAlex

Hydroxypropylemethylecellulose (HPMC) and Polyvinylpyrrolidone (PVP) polymer virgin and blend films were prepared and investigated using wide angle X-ray scattering method. Microstructural parameters like lattice strain (g %), the crystallite size for individual the Bragg’s reflection (hkl) have been computed using line profile analysis and hence by whole pattern fitting method. The X-ray diffraction study reveals that the blending of PVP decreases the crystallanity of HPMC up to 5:4 concentration and then increases. Measured tensile strength decreases, Young’s Modulus decreases, and % elongation increases as the concentration of PVP increases. The surface morphology investigated using scanning electron microscope, shows that the two polymers were miscible in all concentration range.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.007

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.041
GPT teacher head0.357
Teacher spread0.316 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations4
Published2012
Admission routes1
Has abstractyes

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