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Record W2143168801 · doi:10.1073/pnas.1416417112

Heterogeneity of functional groups in a metal–organic framework displays magic number ratios

2015· article· en· W2143168801 on OpenAlexfundno aff
Andrew C.‐H. Sue, Ranjan V. Mannige, Hexiang Deng, Dennis Cao, Cheng Wang, Felipe Gándara, J. Fraser Stoddart, Stephen Whitelam, Omar M. Yaghi

Bibliographic record

VenueProceedings of the National Academy of Sciences · 2015
Typearticle
Languageen
FieldChemistry
TopicMetal-Organic Frameworks: Synthesis and Applications
Canadian institutionsnot available
FundersEnergy Frontier Research CentersNational Center for Research ResourcesNational Institute of General Medical SciencesOffice of ScienceArgonne National LaboratoryU.S. Department of EnergyInternational Institute for Nanotechnology, Northwestern UniversityBasic Energy SciencesKing Abdulaziz City for Science and TechnologyLawrence Berkeley National LaboratoryNorthwestern UniversityYork UniversityUniversity of California, Los AngelesNational Institutes of HealthNational Science Foundation
KeywordsMetal-organic frameworkComponent (thermodynamics)Biological systemMAGIC (telescope)ChemistryNanotechnologyChemical physicsComputer scienceMaterials scienceStatistical physicsTopology (electrical circuits)PhysicsMathematicsThermodynamicsCombinatoricsPhysical chemistryBiology

Abstract

fetched live from OpenAlex

Multiple organic functionalities can now be apportioned into nanoscale domains within a metal-coordinated framework, posing the following question: how do we control the resulting combination of "heterogeneity and order"? Here, we report the creation of a metal-organic framework, MOF-2000, whose two component types are incorporated in a 2:1 ratio, even when the ratio of component types in the starting solution is varied by an order of magnitude. Statistical mechanical modeling suggests that this robust 2:1 ratio has a nonequilibrium origin, resulting from kinetic trapping of component types during framework growth. Our simulations show how other "magic number" ratios of components can be obtained by modulating the topology of a framework and the noncovalent interactions between component types, a finding that may aid the rational design of functional multicomponent materials.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.017
Threshold uncertainty score0.536

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.054
GPT teacher head0.301
Teacher spread0.247 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations38
Published2015
Admission routes1
Has abstractyes

Explore more

Same venueProceedings of the National Academy of SciencesSame topicMetal-Organic Frameworks: Synthesis and ApplicationsFrench-language works237,207