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Record W2160557337 · doi:10.1002/app.25550

Blends of polypropylene with solid silicone additive

2007· article· en· W2160557337 on OpenAlexaff
MA. Patricia Muñoz P., Moisés M. Werlang, Sônia Marlí Bohrz Nachtigall, Nilo Sérgio Medeiros Cardozo, Raquel S. Mauler

Bibliographic record

VenueJournal of Applied Polymer Science · 2007
Typearticle
Languageen
FieldMaterials Science
TopicPolymer crystallization and properties
Canadian institutionsPetro-Canada
Fundersnot available
KeywordsMaterials sciencePolypropyleneDifferential scanning calorimetryCrystallinityPolymer blendVinyltriethoxysilaneRheometryMasterbatchCrystallizationComposite materialChemical engineeringPolymer chemistryCompatibilizationRheologyPolymerSilaneCopolymerNanocompositeThermodynamics

Abstract

fetched live from OpenAlex

Abstract Blends of polypropylene (PP) and silicone masterbatch (SMB PP )—a commercial formulation consisting of an ultrahigh molecular weigh polydimethylsiloxane (PDMS) dispersed in PP—were prepared by melt mixing in an internal mixer. Four binary blends with different SMB PP content and two ternary blends containing silane‐grafted polypropylenes (PP‐VTES) of different VTES content as compatibilizer were produced. The blends were analyzed by melting flow rate, rotational rheometry, scanning electron microscopy, and differential scanning calorimetry (DSC). In all blends, the SMB PP remained as dispersed phase in the continuous PP matrix. The addition of PP‐VTES reduced significantly the size of the SMB PP domains. Rheological and morphological data strongly indicate that the PP‐VTES acts only by lowering the interfacial tension of the system without generating strong interaction between SMB PP domains and the PP matrix. The dimensions of the SMB PP domains and the interfacial energy were observed to determine the characteristics of the pseudoplastic behavior of the blends in the melt state. For both binary and ternary blends, the SMB PP domains showed nucleating effect leading to an increase of the degree of crystallinity. However, the decrease in the interfacial energy and viscosity promoted by the addition of PP‐VTES to the system led to a more intense nucleating effect and to an increase of crystallization, melting temperatures, and melting enthalpy. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 226–233, 2007

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.021
Threshold uncertainty score0.475

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.244
Teacher spread0.235 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations11
Published2007
Admission routes1
Has abstractyes

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