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Record W2162360413 · doi:10.1002/cplu.201500255

Composite Noble‐Metal Films/H<sup>+</sup>‐Conducting Solid‐Polymer Electrolyte Assemblies: The Nitrate‐Reduction Activity in an Asymmetric Sandwich‐Type Reactor

2015· article· en· W2162360413 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueChemPlusChem · 2015
Typearticle
Languageen
FieldChemical Engineering
TopicAmmonia Synthesis and Nitrogen Reduction
Canadian institutionsUniversity of Alberta
FundersThe World Academy of Sciences
KeywordsInorganic chemistryReactivity (psychology)Ternary operationCatalysisElectrochemistryChemistryElectrolyteCathodeHydrogenSelectivityNoble metalMaterials sciencePhysical chemistryElectrodeOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Asymmetric (Pt|Nafion|Pt–Pd–Cu) assemblies were fabricated to study the nitrate‐reduction reaction (NRR) at the cathode surface. The influence of the material composition, supplied current, and applied potential on the reactivity, kinetics, and product selectivity were thoroughly investigated. The cathode assembly consisting of 54 atom % Pt showed enhanced reactivity both in binary (Pt–Pd; k 1 ≈10.7×10 −3 min −1 ) and ternary (Cu–Pt–Pd; k 1 ≈28.6×10 −3 min −1 ) states. This composition was found to be highly nitrite‐selective (80 % in the binary state and 53 % in the ternary state). The mechanistic studies revealed that the reduction of nitrate ions to ammonia proceeded through a catalytic hydrogenation reaction followed by electrochemical hydrogen generation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.026
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.053
GPT teacher head0.282
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it