<i>N,N</i>-Diethyl-<i>N</i>-methyl-<i>N</i>-(methylsulfonyl)ammonium Fluorosulfate
Why this work is in the frame
A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.
Bibliographic record
Abstract
[55791-04-3] C6H16FNO5S2 (MW 265.32) InChI = 1S/C6H16NO2S.FHO3S/c1-5-7(3,6-2)10(4,8)9;1-5(2,3)4/h5-6H2,1-4H3;(H,2,3,4)/q+1;/p-1 InChIKey = VERIHBXWNIYGAA-UHFFFAOYSA-M (reagent for converting, under mild conditions, alcohols into methanesulfonate (mesylate) esters, and primary and secondary amines into methanesulfonamides1, 2) Alternate Name: easy mesyl. Physical Data: mp ∼115 °C (dec).2 Solubility: sol dry MeCN (solutions decompose over a few hours at rt).2 Form Supplied in: not commercially available. Preparative Method: reaction of MeSO2NEt2 with excess neat MeOSO2F at 50 °C for 72 h.2 Analysis of Reagent Purity: 1H NMR (CD3CN) δ: 1.40 (t, 6H), 3.11 (s, 3H), 3.60 (q, 4H), 3.70 (s, 3H).2 Handling, Storage, and Precautions: hygroscopic; hydrolyzed by moist air (products corrosive); stable indefinitely in a sealed ampoule at rt.
Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.001 | 0.001 |
| Meta-epidemiology (narrow) | 0.001 | 0.001 |
| Meta-epidemiology (broad) | 0.002 | 0.001 |
| Bibliometrics | 0.000 | 0.001 |
| Science and technology studies | 0.000 | 0.001 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.002 | 0.001 |
| Research integrity | 0.001 | 0.001 |
| Insufficient payload (model declined to judge) | 0.036 | 0.002 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it