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Theory and simulation of polymerization-induced phase separation in polymeric media

2000· article· en· W2169421178 on OpenAlex
Jungrok Oh, Alejandro D. Rey

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A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueMacromolecular Theory and Simulations · 2000
Typearticle
Languageen
FieldMaterials Science
TopicBlock Copolymer Self-Assembly
Canadian institutionsMcGill University
Fundersnot available
KeywordsDimensionless quantityPolymerizationThermodynamicsPolymerPhase (matter)MonomerDiffusionChemistryPolymer chemistryCondensationMaterials scienceChemical physicsPhysicsOrganic chemistry

Abstract

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A rigorous model of polymerization-induced phase separation (PIPS), based on the non-linear Cahn-Hilliard (C-H) and Flory-Huggins (F-H) theories combined with a second-order polymerization reaction equation, has been formulated and its solutions characterized. The model describes phase separation in system consisting of a non-reactive polymer and a monomer that undergoes condensation polymerization. The model consists of a balance equation for the low molecular weight polymerization regime and another balance equation for the high molecular weight entangled regime. The model equations are solved, and the solutions are characterized to identify the dynamical and morphological phenomena of the PIPS process. The extent of phase separation increases significantly with time during the early stage of phase separation, and slows down in the intermediate stage. The various types of phase-separated morphologies are fully characterized using a novel morphological characterization techniques, known as the intensity and scale of segregation. Both the dynamical and morphological features of the PIPS method are sensitive to the magnitudes of the dimensionless diffusion coefficient D* and the dimensionless reaction rate constant K*. The scale of segregation and the droplet size decreases as D* and K* increase. On the other hand, the intensity of segregation increases with K*, but decreases with D*. The present results extend the present knowledge of the PIPS process by taking into account the effects arising from the presence of a non-reactive polymer.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.097
Threshold uncertainty score0.941

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.292
Teacher spread0.284 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it