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Record W2169911046 · doi:10.1002/jrs.1337

Surface‐enhanced Raman scattering from oxazine 720 adsorbed on scratched gold films

2005· article· en· W2169911046 on OpenAlexafffund
Alexandre G. Brolo, Christopher J. Addison

Bibliographic record

VenueJournal of Raman Spectroscopy · 2005
Typearticle
Languageen
FieldMaterials Science
TopicGold and Silver Nanoparticles Synthesis and Applications
Canadian institutionsUniversity of Victoria
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsRaman scatteringRaman spectroscopyPolarization (electrochemistry)AdsorptionScatteringMaterials scienceElectrodePerpendicularExcitationElectrochemistryAnalytical Chemistry (journal)ChemistryOpticsNanotechnologyPhysical chemistry

Abstract

fetched live from OpenAlex

Abstract Surface‐enhanced Raman scattering (SERS) and surface‐enhanced resonance Raman scattering (SERRS) from oxazine 720 (oxa) dye adsorbed on scratched gold films are reported. The SERS‐active surface was prepared by performing a series of scratches in a 100 nm thick gold film deposited in glass. Atomic force microscopic imaging revealed a sub‐structure within the scratches containing a set of parallel gold wires of different sizes and shapes. The 1‐D order imposed by the parallelism between these wires is responsible for an interesting polarization effect observed in forward scattering experiments. It is shown that the maximum enhanced signal is observed when the polarization of the incident field is perpendicular to the direction of the scratches. This polarization discrimination may be useful in the design of SERS applications in chemical sensing and optical switching. Moreover, we also show that these scratched gold surfaces can be used as ordinary SERS substrates for experiments in backscattering using a common Raman microscope in non‐resonance conditions with the excitation energy. This was accomplished by obtaining the electrochemical SERS of oxa in situ (under electrochemical control). The potential dependence of the SERS from oxa adsorbed on scratched Au is compared with previous results obtained with Ag electrodes. Copyright © 2005 John Wiley & Sons, Ltd.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.260
Teacher spread0.247 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations26
Published2005
Admission routes2
Has abstractyes

Explore more

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