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Record W2288425201 · doi:10.1002/cjce.22464

Transesterification of palm oil in a microtube reactor

2016· article· en· W2288425201 on OpenAlexvenueno aff
Amaraporn Kaewchada, Siriluck Pungchaicharn, Attasak Jaree

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2016
Typearticle
Languageen
FieldEngineering
TopicBiodiesel Production and Applications
Canadian institutionsnot available
FundersCenter of Excellence on Petrochemical and Materials Technology
KeywordsTransesterificationBiodieselMethanolResidence time (fluid dynamics)CatalysisMolar ratioBatch reactorChemistryChemical engineeringFatty acid methyl esterNuclear chemistryMaterials scienceOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Transesterification of palm oil and methanol with KOH as a catalyst in biodiesel synthesis was studied in a microtube reactor. The first part is the investigation on the influences of catalyst amount (5–13 mg/g, 0.5–1.3 mass%), reaction temperature (52–70 °C), methanol‐to‐oil molar ratio (4.5:1–9:1), and residence time (5–20 s) on fatty acid methyl ester content (%FAME). The optimal %FAME of 97.14 % was achieved with the catalyst amount of 10 mg/g (1 mass%), operating at 60 °C, and using a methanol‐to‐oil molar ratio of 6:1 and a residence time of 5 s. High %FAME was obtained at low residence time due to the small size of droplets in the micro‐channel reactor. The second part deals with the effect of mixer and reactor geometry. A comparison between %FAME obtained from the synthesis in a batch stirred‐tank reactor and in a microtube suggested that the reaction proceeded much faster for the latter. The use of a T‐mixer provided superior reaction performance compared to the J‐mixer throughout the conditions studied.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.014
Threshold uncertainty score0.158

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.175
Teacher spread0.165 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations22
Published2016
Admission routes1
Has abstractyes

Explore more

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