Liquid–Liquid Mass Transfer in an Oscillatory-Flow Mesoscale Coil Reactor without Baffles
Bibliographic record
Abstract
Interphase mass transfer rates of an immiscible liquid–liquid system are investigated in an oscillatory-flow coil reactor without baffles. A baffle-less system is chosen since much research has been completed in baffled tubes with little performance comparison to baffle-less tubes, which offer lower operating and capital costs. In our experiments, interphase mass transfer rates are evaluated via the two-phase alkaline hydrolysis of 4-nitrophenyl acetate (4-NPA) in a toluene–water biphasic system. The mass transfer rate increased 7-fold at the maximum tested oscillation of 5000 oscillatory-flow Reynolds number. The best application for the oscillatory-flow coil reactor is determined using a comparison to other liquid–liquid flow platforms in the presented toolbox approach. The oscillatory-flow coil reactor becomes a clear complement to a plate microreactor for gaining volume.
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How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.000 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".