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Record W2315036368 · doi:10.1021/cm402593f

Enhanced Thermoelectric Properties of Variants of Tl<sub>9</sub>SbTe<sub>6</sub> and Tl<sub>9</sub>BiTe<sub>6</sub>

2013· article· en· W2315036368 on OpenAlexaff
Quansheng Guo, Meghan Chan, Bryan A. Kuropatwa, Holger Kleinke

Bibliographic record

VenueChemistry of Materials · 2013
Typearticle
Languageen
FieldMaterials Science
TopicAdvanced Thermoelectric Materials and Devices
Canadian institutionsUniversity of Waterloo
Fundersnot available
KeywordsSeebeck coefficientThermoelectric effectThermoelectric materialsMaterials scienceElectrical resistivity and conductivityIsostructuralThermal conductivityHot pressingCharge carrierAnalytical Chemistry (journal)SemiconductorCondensed matter physicsMetallurgyOptoelectronicsThermodynamicsComposite materialCrystallographyChemistryCrystal structurePhysics

Abstract

fetched live from OpenAlex

Tl 9 BiTe 6, a substitution variant of Tl 5 Te 3, is one of the leading midtemperature thermoelectrics and is postulated to exceed ZT = 1 above 450 K when prepared by zone-melting and reach ZT = 0.86 at 560 K after hot-pressing. We have prepared the isostructural series Tl 9 Sb 1– x Te 6, Tl 9– x Sb 1+ x Te 6, Tl 9 Bi 1– x Te 6, and Tl 9– x Bi 1+ x Te 6, with x ranging from 0 to 0.05, from the elements in the stoichiometric ratios and determined their thermoelectric properties after hot-pressing. In theory, these tellurides are narrow-gap semiconductors when x = 0, with all elements in common oxidation states, according to (Tl + ) 9 (Sb/Bi) 3+ (Te 2– ) 6 . The as-prepared samples of this 9-1-6 stoichiometry, however, exhibit relatively high electrical conductivity, which decreases with increasing temperature, indicative of the presence of extrinsic charge carriers. The Seebeck coefficient is generally above +100 μV K –1 . Decreasing the Sb and Bi content increases the hole carrier concentration and thus increases the electrical conductivity while decreasing the Seebeck coefficient. The best feature of these thermoelectrics is their low thermal conductivity, which is consistently well below 0.7 W m –1 K –1 . In combination with reasonable electrical conductivity and a high Seebeck coefficient, high ZT values in excess of 1 can also be achieved via simple hot-pressing after experimental optimization of the carrier concentration via introducing deficiencies on the Bi site. Moreover, the variants with Sb instead of Bi exhibit similar thermoelectric performance, a result of the combination of a better electrical performance and higher thermal conductivity.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.198
Teacher spread0.189 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations70
Published2013
Admission routes1
Has abstractyes

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