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Record W2318076649 · doi:10.1021/ie501673v

Enhanced Solar Photocatalytic Degradation of Phenol with Coupled Graphene-Based Titanium Dioxide and Zinc Oxide

2014· article· en· W2318076649 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2014
Typearticle
Languageen
FieldEnergy
TopicAdvanced Photocatalysis Techniques
Canadian institutionsUniversity of WaterlooDalhousie UniversityWestern University
Fundersnot available
KeywordsPhotocatalysisTitanium dioxideMaterials scienceGrapheneRaman spectroscopyX-ray photoelectron spectroscopyChemical engineeringPhenolScanning electron microscopeZincOxideNuclear chemistryCatalysisComposite materialChemistryNanotechnologyOrganic chemistryOptics

Abstract

fetched live from OpenAlex

In this study, graphene-based titanium dioxide and zinc oxide composites (TiO 2 -G, ZnO-G) were synthesized using a hydrothermal process. Materials were characterized using X-ray diffraction, X-ray photoelectron spectroscopy, Raman spectroscopy, UV–vis spectroscopy, scanning electron microscopy, and transmission electron microscopy. Photocatalytic activity of the composite materials under simulated solar light was studied using phenol as a model compound. A ca. 30% improvement on the degradation performance by the TiO 2 -G composite (and ZnO-G) was observed when reaction rate constants were compared with TiO 2 (and ZnO) only. This demonstrates the positive effect of graphene on suppressing charge recombination and extending the light absorption range. Further improvement on the photocatalytic degradation rate of phenol was obtained by coupling the two composites, ZnO-G and TiO 2 -G. This is attributed to more efficient charge separation and longer lifetime of the charge carriers, which eventually enhances the photocatalytic activity. The optimum stoichiometric amount of each component was obtained experimentally. Systematic parametric studies were also performed to study the effect of catalyst loading, initial phenol concentration, solution pH, and solar light intensity. Complete solar degradation of 40 ppm phenol was achieved within 60 min while using the coupled ZnO-G/TiO 2 -G photocatalysts at the optimum conditions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.020
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.032
GPT teacher head0.288
Teacher spread0.255 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it