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Record W2320850963 · doi:10.1107/s0108767311083620

Hybrid inorganic–organic layered crystals constructed by oxide clusters and surfactant

2011· article· en· W2320850963 on OpenAlexaffabout
Takeru Ito, Keisuke Mikurube, Kan-ichi Hasegawa, Mariko Kurasawa, Haruo Naruke, Tomoji Ozeki

Bibliographic record

VenueActa Crystallographica Section A Foundations of Crystallography · 2011
Typearticle
Languageen
FieldChemical Engineering
TopicCatalysis and Oxidation Reactions
Canadian institutionsCanadian Museum of NatureUniversity of ManitobaGeological Survey of Canada
Fundersnot available
KeywordsPulmonary surfactantOxideChemical engineeringMaterials scienceNanotechnologyMetallurgy

Abstract

fetched live from OpenAlex

Veblenite, ideally KNa(Fe 2+ 5 Fe 3+ 4 Mn 7 )Nb 4 (Si 2 O 7 ) 2 (Si 8 O 22 ) 2 O 6 (OH) 10 (H 2 O) 3 , triclicnic, P1, a 5.3761(3), b 27.5062(11), c 18.6972(9) , 140.301(3), 93.033(3), 95.664(3) , V 1720.96(14) 3 , has no natural or synthetic analogues. It is a new mineral occurring at Ten Mile Lake, Seal Lake area, Labrador, Newfoundland, Canada, as red brown single laths and fibres included in feldspar. In the crystal structure of veblenite, M octahedra share common edges to form a wavy octahedral sheet parallel to (001). SiO 4 tetrahedra share corners to form Si 2 O 7 groups and Si 8 O 22 ribbons. This is the first occurrence of an eightmembered Si-O ribbon in a mineral crystal structure. The Nb-dominant D octahedra, Si 2 O 7 groups and Si 8 O 22 ribbons share common vertices to form a heteropolyhedral (H) sheet. Two H sheets and an O sheet constitute an HOH block. Along [001], HOH blocks connect via common vertices of D octahedra and cations at the A(1,2) and B interstitial sites. In the intermediate space between two adjacent HOH blocks, two [100] channels of different size can be identified. A narrow channel of the width of an Si 2 O 7 group contains the A(1) site mainly occupied by K. A large channel has the width of four Si 2 O 7 groups (Si 8 O 22 ribbon) and contains A(2) sites partly occupied by K and H 2 O groups.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.633
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.002
Science and technology studies0.0000.001
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.209
Teacher spread0.198 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2011
Admission routes2
Has abstractyes

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