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Preparation and comprehensive characterization of a calcium hydroxyapatite reference material

2004· article· en· 447 citations· W2323613579 on OpenAlex· 10.6028/jres.109.042

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A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

Canadian funderA Canadian agency funded it. The work may carry no Canadian affiliation at all.

No Canadian affiliation. An affiliation-only frame — the usual design — would never have seen this work. It is one of the works that make the case for inverting the frame.

Machine scores (provisional)

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Opus teacher head0.042
GPT teacher head0.355
Teacher spread
0.313 · how far apart the two teachers sit on this one work
Validation status
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Abstract

Numerous biological and chemical studies involve the use of calcium hydroxyapatite (HA), Ca10(PO4)6(OH)2. In this study detailed physicochemical characterization of HA, prepared from an aqueous solution, was carried out employing different methods and techniques: chemical and thermal analyses, x-ray diffraction, infrared and Raman spectroscopies, scanning and transmission microscopies, and Brunauer, Emmett, and Teller (BET) surface-area method. The contents of calcium (Ca(2+)), phosphate (PO4 (3-)), hydroxide (OH(-)), hydrogenphosphate (HPO4 (2-)), water (H2O), carbonate (CO3 (2-)), and trace constituents, the Ca/P molar ratio, crystal size and morphology, surface area, unit-cell parameters, crystallinity, and solubility of this HA were determined. This highly pure, homogeneous, and highly crystalline HA is certified as a National Institute of Standards and Technology (NIST) standard reference material, SRM 2910.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

The record

Venue
Journal of Research of the National Institute of Standards and Technology
Topic
Bone Tissue Engineering Materials
Field
Engineering
Canadian institutions
Funders
National Institute of Dental and Craniofacial ResearchNational Institute of Standards and TechnologyNorth Dakota State UniversityNational Institutes of HealthUniversity of TorontoADA Foundation
Keywords
CrystallinityMaterials scienceAqueous solutionSolubilityRaman spectroscopyCharacterization (materials science)MineralogyBioceramicChemical engineeringSpecific surface areaHydroxyapatitesCertified reference materialsNuclear chemistryCalciumAnalytical Chemistry (journal)ChemistryNanotechnologyChromatographyComposite materialPhysical chemistryOrganic chemistry
Has abstract in OpenAlex
yes