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Record W2324715524 · doi:10.3998/ark.5550190.0002.c17

Investigation of the mechanism of 1,2-migrations in methoxysiloxycarbene with the electron localization function

2002· article· en· W2324715524 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueARKIVOC · 2002
Typearticle
Languageen
FieldChemistry
TopicOrganometallic Complex Synthesis and Catalysis
Canadian institutionsConcordia University
FundersNatural Sciences and Engineering Research Council of CanadaConcordia University
KeywordsCarbeneChemistryLone pairSilylationValence (chemistry)NucleophileElectron localization functionElectronCatalysisMoleculeOrganic chemistryPhysicsQuantum mechanics

Abstract

fetched live from OpenAlex

A topological analysis of the gradient vector field of the electron localization function (ELF) has been used to investigate the mechanism of 1,2-silyl migration from oxygen to the carbene carbon in methoxysiloxycarbene. As well, the analogous 1,2-methyl migration was investigated for comparison. Plots of ELF isosurfaces and contour maps clearly reveal that the monosynaptic valence basin corresponding to the carbene lone pair becomes the disynaptic valence basin corresponding to the developing carbon-silicon bond in the transition state for 1,2-silyl migration, while it remains effectively unaltered in the transition state for 1,2-methyl migration. These results suggest that 1,2-silyl migration proceeds via nucleophilic attack by the carbene lone pair at silicon, whereas the energetically unfavorable 1,2-methyl migration appears to involve an anion-like shift from oxygen to the carbene center, in good agreement with previous findings.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.017
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.186
Teacher spread0.170 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it