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Record W2330812121 · doi:10.1021/ef200977p

Experimental and Modeling Study of Trends in the High-Temperature Ignition of Methyl and Ethyl Esters

2011· article· en· W2330812121 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueEnergy & Fuels · 2011
Typearticle
Languageen
FieldChemical Engineering
TopicAdvanced Combustion Engine Technologies
Canadian institutionsMcGill University
Fundersnot available
KeywordsChemistryEthyl formateReactivity (psychology)Ethyl acetateMethyl formateMethyl acetateOrganic chemistryEthyleneIgnition systemEthanolMethanolCatalysisThermodynamics

Abstract

fetched live from OpenAlex

Methyl and ethyl esters of carboxylic acids can be obtained from the trans-esterification of fatty acid triglycerides using methanol and ethanol, respectively. In this work, the relative ignition of methyl and ethyl esters is reported, based on new high-temperature shock tube ignition data of ethyl acetate (EA) and ethyl propanoate (EP). These are compared with literature data for other methyl and ethyl esters, and isomer and alkyl group effects are also investigated. It is found that ethyl esters are generally characterized by shorter ignition delay times than those of methyl esters of the corresponding alkanoic acid. Increased reactivity of ethyl esters is also observed for isomeric ethyl and methyl esters. A combined high-temperature chemical kinetic model is proposed for methyl and ethyl acetates as well as for ethyl formate in order to shed light on the link between chemical structure and the observed reactivity trends. The proposed model reflects the experimental trends and generally predicts ignition delay times in close agreement with measured data. The reduced methyl acetate reactivity is attributed both to the absence of more reactive secondary C–H sites and the ethyl group which facilitates complex unimolecular decomposition reactions in ethyl esters such as acid and ethylene elimination. The model and the new experimental data contribute toward improved understanding and modeling of the combustion properties of biodiesel surrogates.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.295

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.030
GPT teacher head0.258
Teacher spread0.228 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it