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Record W2331619376 · doi:10.1021/ie4006589

Steady-State Simulation of a Novel Annular Multitubular Reactor for Enhanced Methanol Production

2013· article· en· W2331619376 on OpenAlexaff
Abdulaziz Alarifi, Ali Elkamel, Eric Croiset

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2013
Typearticle
Languageen
FieldChemical Engineering
TopicCatalysts for Methane Reforming
Canadian institutionsUniversity of Waterloo
Fundersnot available
KeywordsMethanolSyngasExothermic reactionAir preheaterChemical engineeringCatalysisMethanol reformerMaterials scienceChemistrySteam reformingOrganic chemistryHydrogen production

Abstract

fetched live from OpenAlex

In this study, a one-dimensional heterogeneous model with intraparticle diffusion limitation has been developed for methanol synthesis from syngas. The synthesis gas produced from the reformer is compressed at a pressure of 60–100 bar and then heated up to 200–250 °C in order to prepare it for the methanol production reaction. Syngas reacts on a copper oxide/zinc oxide/alumina catalyst. The annular multitubular (AMT) reactor proposed in this article has a design capability to efficiently remove the heat generated by the exothermic reaction in methanol synthesis and improve methanol production by at least 3% more than the conventional converter. In addition, the converter is operated under mild conditions, especially at the end of the tube, which makes the catalyst lasts for a longer period. This leads to process intensification and allows for the use of a compact distillation step. In addition, this new design has the advantage of preheating the feed gas in the reaction by having the inner tubes replace the feed gas preheater. Methanol production and temperature profile are the most important characteristics of methanol synthesis reactor. The predicted methanol concentration and temperature profile indicate that an increase in temperature is accompanied with a reduction in the methanol equilibrium concentration and hence limiting the profitability in the industrial plant. The use of an AMT reactor is shown to be able to overcome this limitation. The novelty lies in a process modification which employs an inner tube that is disposed in the reactor and then the catalyst is charged into a circular space surrounded by the reaction tube on one side and inner tube on the other side. Simulation studies show that this design allows the temperature to increase gradually and, hence, delays the equilibrium to be reached to the end of the reactor. In other words, more methanol is produced and less byproducts.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.006
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.006
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.102
GPT teacher head0.349
Teacher spread0.247 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations12
Published2013
Admission routes1
Has abstractyes

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