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Record W2333995721 · doi:10.1021/jp4024734

First-Principles Investigation of Selective Oxidation of Propane on Clean and Sulfided V<sub>2</sub>O<sub>5</sub> (010) Surfaces

2013· article· en· W2333995721 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2013
Typearticle
Languageen
FieldChemical Engineering
TopicCatalysis and Oxidation Reactions
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsDehydrogenationPropanePropeneChemistryActivation energyCatalysisDesorptionReaction mechanismDensity functional theoryLattice energyPhysical chemistryKinetic energyInorganic chemistryCrystallographyAdsorptionCrystal structureComputational chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Oxidative dehydrogenation of propane on single-crystal V 2 O 5 and V 2 O 4 S surfaces has been studied by means of periodic density functional theory. Three previously proposed ODH reaction mechanisms, namely the multisite vanadyl mechanism, the vanadyl-lattice mechanism, and the multisite bridging mechanism, were investigated. Results were compared with existing data from the literature. It was found that the multisite vanadyl mechanism plays the most dominant role in propene formation, with an apparent activation energy of 27 kcal/mol, in very good agreement with the experimental value. The present study also demonstrated that the other two mechanisms are less important in the propane ODH reaction because of the kinetic hindrance arising from the H 2 O desorption and O 2 addition at the lattice site. On the other hand, the effects of sulfur substituents on V 2 O 5 are detrimental in general. In the presence of H 2 S, V 2 O 5 could be readily sulfided, with the estimated activation energy of 30 kcal/mol and reaction energy of 2.5 kcal/mol. At moderate temperatures, a small amount of surface V═O will be converted to V═S, which raises the apparent activation energy associated with the multisite vanadyl mechanism by only 3 kcal/mol. Further increase of reaction temperatures, however, would lead to the formation of lattice S whose accumulation results in the deactivation of the catalyst.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.007
Threshold uncertainty score0.460

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.207
Teacher spread0.195 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it