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Record W2333997631 · doi:10.1021/jp400132k

The Protein Environment of the Bacteriopheophytin Anion Modulates Charge Separation and Charge Recombination in Bacterial Reaction Centers

2013· article· en· W2333997631 on OpenAlexafffund
Jie Pan, Rafael G. Saer, Su Lin, Zhi Guo, J. Thomas Beatty, Neal W. Woodbury

Bibliographic record

VenueThe Journal of Physical Chemistry B · 2013
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicPhotosynthetic Processes and Mechanisms
Canadian institutionsUniversity of British Columbia
FundersDivision of Molecular and Cellular BiosciencesNatural Sciences and Engineering Research Council of Canada
KeywordsPhotosynthetic reaction centreChemistryRhodobacter sphaeroidesElectron transferKineticsMethionineLeucinePhotochemistryAlanineAmino acidBiochemistryPhotosynthesis

Abstract

fetched live from OpenAlex

The kinetics and pathway of electron transfer has been explored in a series of reaction center mutants from Rhodobacter sphaeroides, in which the leucine residue at M214 near the bacteriopheophytin cofactor in the A-branch has been replaced with methionine, cysteine, alanine, and glycine. These amino acids have substantially different volumes, both from each other and, except for methionine, from the native leucine. Though the mutation site of M214 is close to the bacteriopheophytin cofactor, which is involved in the electron transfer, none of the mutations alter the cofactor composition of the reaction center and the primary charge separation reaction is essentially undisturbed. However, the kinetics of electron transfer from HA(-) → QA becomes both slower and substantially heterogeneous in three of the four mutants. The decreased HA(-) → QA electron transfer rate allows charge recombination between P(+) and HA(-) to compete with the forward reaction, resulting in a drop in the overall yield of charge separation. Both the yield change and the variation in kinetics correlate well with the volume of the mutant amino acid side chains. Analysis of the kinetics suggests that the introduction of a smaller side chain at M214 results in greater protein structural heterogeneity and dynamics on multiple time scales, resulting in perturbation of the electronic environment and its evolution in the vicinity of the early charge-separated radical pair, P(+)HA(-), and the subsequent acceptor QA, affecting both the extent and time scale of dielectric relaxation. It appears that the reaction center has been optimized not only in terms of its static structure-function relationships, but also finely tuned to favor particular reaction pathways on particular time scales by adjusting protein dynamics.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.200
Teacher spread0.196 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations17
Published2013
Admission routes2
Has abstractyes

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