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Record W2342149806 · doi:10.1149/ma2014-01/7/496

Study of Carbon Formed on Stainless Steel 304H in a Simulated Environment of the Convection Section of the Ethane Cracking Furnace System

2014· article· en· W2342149806 on OpenAlexaff
Farshid Ramezanipour, Anand Singh, Scott Paulson, Hany Farag, Viola Birss, Venkataraman Thangadurai

Bibliographic record

VenueECS Meeting Abstracts · 2014
Typearticle
Languageen
FieldMaterials Science
TopicHydrogen embrittlement and corrosion behaviors in metals
Canadian institutionsNova Chemicals (Canada)University of Calgary
Fundersnot available
KeywordsCrackingCarbon fibersMaterials scienceScanning electron microscopeChemisorptionAlloyCarburizingPetrochemicalEthyleneChemical engineeringMetallurgyChemistryComposite materialCatalysisOrganic chemistry

Abstract

fetched live from OpenAlex

The stainless steel 304H (SS304H) is one of the important alloys used in petrochemical industry, such as in the convection section of the ethylene production furnaces. The exposure to carburizing gases makes this alloy susceptible to carbon formation and potential carburization. The present study focuses on understanding the coking behavior of SS304H in ethane/steam environment and the effect of H 2 S at 700 o C. Long-term (90 hours) experiments in such environment show that the addition of ppm amounts of H 2 S has a pronounced effect on the morphology of the carbon formed on the SS304H surface, as shown by scanning electron microscopy. In the absence of H 2 S, the deposited carbon forms distinct fibers, which are distributed homogeneously on the surface. The addition of 15 ppm H 2 S results in the formation of carbon clusters, consisting of very thin fibers that are tightly entangled. Also, experiments in the presence of H 2 S showed a systematic decrease in the amount of carbon as H 2 S increased from 1 to 2, 5, 7, and 10 ppm. At 10 ppm H 2 S, no carbon was observed on the SS304H surface after 4 h of exposure to ethane/steam at 700 o C. Mass spectrometry studies showed that the addition of H 2 S does not affect the temperature or products of ethane cracking. The effect of the SS304H coupons on the ethane cracking products was also studied by mass spectrometry, and showed that the ethane cracking process is not significantly affected by the presence of the metal coupon.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.156
Threshold uncertainty score0.346

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.246
Teacher spread0.228 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2014
Admission routes1
Has abstractyes

Explore more

Same venueECS Meeting AbstractsSame topicHydrogen embrittlement and corrosion behaviors in metalsFrench-language works237,207