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Record W2365596174

Simultaneous determination of four main constituents in Xuefuzhuyu pills

2008· article· en· W2365596174 on OpenAlexaff
Dan Li

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldMedicine
TopicTraditional Chinese Medicine Analysis
Canadian institutionsCAE (Canada)
Fundersnot available
KeywordsChemistryChromatographyPaeoniflorinFerulic acidHesperidinAcetic acidGradient elutionHigh-performance liquid chromatographyAcetonitrileLinear rangeDetection limit
DOInot available

Abstract

fetched live from OpenAlex

Objective:To simultaneous determination of four main components in Xuefuzhuyu pills by HPLC meth- od.Method:The separation of four ingredients was achieved on a Kromasil ODS C_(18) column (250 mm×4.6 mm,5 μm) with gradient elution by mixture of acetonitrile -0.25% acetic acid.The flow rate was 1.0 mL·min~(-1) and the detective wavelength was 265 nm.Result:Assay was linear over the range of 23.85-119.3 μg·mL~(-1) for hydro- safflor yellow A,140 -644μg·mL~(-1) for paeoniflorin,10.25-47.15 μg·mL~(-1) for ferulic acid,and 130-598 μg ·mL~(-1) for hesperidin respectively.Average recoveries of samples were all over 96.6%,RSD were all below 2.0%.Conclusion:The method is simple and accurate.It provides method of quality assessment of Xuefuzhuyu pills.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: Observational
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.067
Threshold uncertainty score0.379

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.027
GPT teacher head0.277
Teacher spread0.250 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designObservational
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2008
Admission routes1
Has abstractyes

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