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Record W2402440006 · doi:10.1021/acs.iecr.5b03412

Analysis of Reaction Kinetics of CO<sub>2</sub> Absorption into a Novel 1-(2-Hydroxyethyl)-piperidine Solvent Using Stopped-Flow Technique

2015· article· en· W2402440006 on OpenAlexaff
Helei Liu, Min Xiao, Zhiwu Liang, Wichitpan Rongwong, Jie Li, Paitoon Tontiwachwuthikul

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2015
Typearticle
Languageen
FieldEngineering
TopicCarbon Dioxide Capture Technologies
Canadian institutionsUniversity of Regina
FundersMinistry of Science and Technology of the People's Republic of ChinaMinistry of Education of the People's Republic of ChinaNational Natural Science Foundation of China
KeywordsPiperidineKineticsChemistryReaction rate constantAqueous solutionAbsorption (acoustics)SolventBase (topology)Chemical kineticsThermodynamicsReaction mechanismAnalytical Chemistry (journal)CatalysisPhysical chemistryStereochemistryChromatographyOrganic chemistryMaterials science

Abstract

fetched live from OpenAlex

In this present work, the absorption kinetics of CO 2 into aqueous 1-(2-Hydroxyethyl) piperidine (1-(2-HE)PP) solutions with respect to observed pseudo-first-order rate constant ( k 0 ) and second order reaction rate constant ( k 2 ), were determined using the stopped-flow apparatus within the 1-(2-HE)PP concentration range of 0.20–1.00 kmol/m 3 and a temperature range of 293–313 K. The values of k 0 were then represented using the correlation based on the base-catalyzed hydration mechanism. The results show that the correlated values of k 0 matched well with the experimental values with an acceptable AAD of 8.3%, which indicates that the base-catalyzed hydration mechanism can satisfactorily describe the experimental kinetics data of the1-(2-HE)PP reaction with CO 2 . In order to comprehensively understand the kinetics, the ion speciation plots of 1-(2-HE)PP-H 2 O–CO 2 system were developed using the pH method. In addition, the Brønsted plots between k 2 (obtained from stopped-flow apparatus) and p K a (obtained from experimental measurement) for 1-(2-HE)PP were developed, and then used to predict k 2 using the values of p K a .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.092
GPT teacher head0.319
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations17
Published2015
Admission routes1
Has abstractyes

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