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Record W2414918391 · doi:10.1385/1-59259-184-1:057

Fourier Transform Infrared Spectroscopy of Calcium-Binding Proteins

2003· article· en· W2414918391 on OpenAlexaff
Heinz Fabian, Hans J. Vogel

Bibliographic record

VenueHumana Press eBooks · 2003
Typearticle
Languageen
FieldChemistry
TopicMass Spectrometry Techniques and Applications
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsFourier transform infrared spectroscopyInfraredInfrared spectroscopyChemistryFourier transformSpectroscopyAnalytical Chemistry (journal)Protein structureCrystallographyOpticsChromatographyPhysicsBiochemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Infrared spectroscopy measures absorptions of vibrating molecules and yields information about molecular structure and structural interactions. Over the last two decades, the infrared technique has emerged as a very useful tool for examining protein conformation as a result of the increase in energy throughput, achievable signal-to-noise ratio, wavenumber accuracy, and data aquisition rates that came with the development of Fourier transform infrared (FTIR) spectrometers. High-quality infrared spectra can now rapidly be aquired and require only relatively small amounts of protein. The size of the protein or the nature of the environment does not limit the application of FTIR spectroscopy. Importantly, measurements of proteins in aqueous solution are almost routine now. Furthermore, the process of obtaining structural information is not restricted to a static picture, but can also be achieved in real time by applying time-resolved infrared techniques. The effects of environmental factors, point mutations, or ligand binding on the structure of the proteins can be examined with high sensitivity by using peptide backbone and side-chain infrared bands as conformation-sensitive monitors. In combination with isotope labeling, the technique also permits the study of protein-protein or protein-peptide interactions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Other · Consensus signal: none
Teacher disagreement score0.923
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.044
GPT teacher head0.292
Teacher spread0.248 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations12
Published2003
Admission routes1
Has abstractyes

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