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Record W2416827673 · doi:10.2138/am-2001-2-310

Al,Si order in the crystal structure of α-eucryptite (LiAlSiO <sub>4</sub> )

2001· article· en· W2416827673 on OpenAlexaff
P. Daniels, Colin A. Fyfe

Bibliographic record

VenueAmerican Mineralogist · 2001
Typearticle
Languageen
FieldChemistry
TopicAdvanced NMR Techniques and Applications
Canadian institutionsUniversity of British Columbia
FundersAlexander von Humboldt-StiftungV Foundation for Cancer Research
KeywordsAcentric factorCrystal structureCrystallographySiliconDiffractionCrystal (programming language)SpectroscopySingle crystalOrder (exchange)Materials scienceChemistryPhysicsOptics

Abstract

fetched live from OpenAlex

The crystal structure of α-eucryptite, LiAlSiO4, is reinvestigated by combining 29Si NMR spectroscopy and single-crystal X-ray diffraction. The silicon coordination in α-eucryptite of three different samples (two of natural, one of synthetic origin) is shown to be identical on a local scale by means of 29Si MAS NMR spectroscopy. This method also suggests a well ordered arrangement of Si and Al within the crystal structure of α-eucryptite and the presence of two symmetrically non-equivalent sites for silicon. The refinement of the structure of a natural crystal using single-crystal X-ray diffraction confirms these observations and demonstrates the presence of long-range Al-Si order and the acentric space group R3.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.434
Threshold uncertainty score0.509

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.274
Teacher spread0.264 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations19
Published2001
Admission routes1
Has abstractyes

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