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Record W2435630042 · doi:10.1385/1-59745-167-3:31

Assay of Dolichyl-Phospho-Mannose Synthase Reconstituted in a Lipid Matrix

2006· article· en· W2435630042 on OpenAlexaff
John S. Schutzbach

Bibliographic record

VenueHumana Press eBooks · 2006
Typearticle
Languageen
FieldChemistry
TopicCarbohydrate Chemistry and Synthesis
Canadian institutionsQueen's University
FundersNational Institute of General Medical SciencesNational Institutes of HealthNational Cancer InstituteNational Institute for Health and Care Research
KeywordsMembraneEndoplasmic reticulumEnzymeBiochemistryGolgi apparatusMannoseGlycolipidChemistryGlycosyltransferaseMembrane proteinGlycoproteinPhospholipidPeripheral membrane proteinIntegral membrane protein

Abstract

fetched live from OpenAlex

Advances in molecular biology over the last several decades, along with new highly developed methods for protein expression, have enabled investigators to produce and purify large yields of the soluble protein domains of a number of eukaryotic glycosyltransferases and processing glycosidases. The availability of these purified enzymes has in turn allowed determination of the crystal structures of the catalytic domains of some of the proteins, thus providing details of the active site geometry and catalytic mechanisms of the enzymes. It must be remembered, however, that the natural subcellular locations for enzymes involved in glycoprotein and glycolipid synthesis are the membranes of the endoplasmic reticulum and Golgi, where the enzymes exist bound to or inserted in the membrane matrix. Because of technical difficulties, few of the intact enzymes containing their hydrophobic membrane-interactive domains have been purified and studied in a membrane environment, even though the membrane has been shown to have effects on the properties and kinetics of many enzymes. Therefore, a method for the reconstitution of dolichyl-phospho-mannose (Dol-P-Man) synthase in phospholipids and phospholipid membranes will be described in detail. In order to properly characterize membrane glycosyltransferases and glycosidases, it is necessary to investigate the kinetic and catalytic properties of these proteins in a membrane environment. The ultimate goal is to define the topography of the proteins in membranes and also to understand the kinetic and catalytic properties of these enzymes in biological membranes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.433
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.025
GPT teacher head0.254
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2006
Admission routes1
Has abstractyes

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