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Record W2462220242 · doi:10.1002/cplu.201600228

Emissive Heterobimetallic Copper(I) Dicyanoaurate‐Based Coordination Polymers

2016· article· en· W2462220242 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueChemPlusChem · 2016
Typearticle
Languageen
FieldChemistry
TopicMetal-Organic Frameworks: Synthesis and Applications
Canadian institutionsSimon Fraser University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsTetrahydrothiophenePyridineCrystallographyChemistryCopperPhotoluminescenceLigand (biochemistry)PolymerExcited stateStereochemistryMaterials scienceOptoelectronicsPhysicsOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Five new Cu I /[Au(CN) 2 ] − ‐based coordination polymer materials—Cu(py) 2 [Au(CN) 2 ] ( 1 ), Cu(PPh 3 )(MeCN)[Au(CN) 2 ] ⋅ MeCN ( 2 a ), Cu(PPh 3 )(MeCN)[Au(CN) 2 ] ( 2 b ), Cu 3 (THT) 4 [Au(CN) 2 ] 3 ( 3 a ) and Cu(THT)[Au(CN) 2 ] ( 3 b )—were prepared and characterized in terms of their structural and photoluminescence properties, and thermal stability (py=pyridine, THT=tetrahydrothiophene). While 1 and 2 a / 2 b adopted one‐dimensional zig‐zag chain structures with no Au ⋅⋅⋅ Au (aurophilic) bonding, 3 a and 3 b exhibited much more complex three‐dimensional frameworks featuring numerous aurophilic interactions; bridging THT units formed either eight‐membered Cu 4 S 4 rings ( 3 a ) or helical (Cu/S) n chains ( 3 b ). When these materials are excited using a broad‐band UV source (365 nm), they each emit light of a distinct colour (except for 2 a ): light green for 1 , pale blue for 2 b , deep blue for 3 a , and violet for 3 b ( λ max =506 nm ( 1 ), 464 nm ( 2 b ), 457 nm ( 3 a ) and 404 nm ( 3 b )). The emission band in 1 , 2 b and 3 b was assigned to Cu I /ligand/CN − ‐based MLCT transitions, while the emission band of 3 a appears to be influenced by the presence of the aurophilic interactions in the structure. Materials 1 and 3 a lose their bound pyridine and THT, respectively, at 110 and 95 °C, respectively, indicating their potential utility as sensory materials.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.062
Threshold uncertainty score0.989

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0120.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.247
Teacher spread0.228 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it