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Record W2481096479 · doi:10.1021/bk-2012-1092.ch003

Effect of Metal Ions on Light Gas Oil Upgrading over Nano Dispersed MoS<sub>x</sub>Catalysts Using<i>in Situ</i>H<sub>2</sub>

2012· book-chapter· en· W2481096479 on OpenAlexafffundabout
Lei Jia, Flora T. T. Ng

Bibliographic record

VenueACS symposium series · 2012
Typebook-chapter
Languageen
FieldEngineering
TopicCatalysis and Hydrodesulfurization Studies
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaSaudi Aramco
KeywordsCatalysisMaterials scienceIonNano-MetalIn situMetal ions in aqueous solutionNanotechnologyAnalytical Chemistry (journal)Chemical engineeringInorganic chemistryMetallurgyComposite materialChemistryEnvironmental chemistryOrganic chemistryEngineering

Abstract

fetched live from OpenAlex

Hot water extraction and steam injection techniques are used to recover the bitumen from the oil sands or from deep underground deposits generating bitumen emulsions. A novel one-step bitumen upgrading process was developed in our laboratory where the water in the bitumen emulsion was activated through the water gas shift reaction (WGSR) to provide in situ H2 for hydrodesulfurization (HDS) and upgrading of the bitumen. The catalyst precursor, phosphomolybdic acid, was transformed into a nano dispersed Mo sulfide catalyst in situ during the upgrading reaction. This nano dispersed Mo catalyst was found to be effective for upgrading light gas oil (LGO) derived from Alberta oil sands with in situ H2. The effect of Ni, Co, Fe, V and K on the nano dispersed Mo sulfide catalyst for the upgrading of LGO was investigated. Ni, Co promoted both WGSR and HDS. V and K inhibited HDS although they promoted WGSR. Fe showed no significant effect on either WGSR or HDS. Ni was found to be the best promoter for HDS. Atthough K was the best promoter for WGSR, however, K apparently inhibited HDS completely but did not affect the boiling point distribution of the oil product. The effects of water content, syn-gas composition and reaction temperature were also discussed. Extra water inhibited HDS when usingeither in situ H2 or molecular H2. Syn-gas could be used for providing in situ H2 for LGO upgrading. Higher reaction temperature favoured both HDS and hydrocracking.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.052
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.203
Teacher spread0.196 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2012
Admission routes3
Has abstractyes

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