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Record W2485863535 · doi:10.1021/bk-2003-0838.ch019

Exploiting Favorable Silicone—Protein Interactions: Stabilization against Denaturation at Oil—Water Interfaces

2003· book-chapter· en· W2485863535 on OpenAlexafffund
Paul M. Zelisko, Vasiliki Bartzoka, Michael A. Brook

Bibliographic record

VenueACS symposium series · 2003
Typebook-chapter
Languageen
FieldMaterials Science
TopicPolymer Surface Interaction Studies
Canadian institutionsMcMaster University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsEmulsionDenaturation (fissile materials)Silicone oilChemistryAqueous solutionAqueous two-phase systemBovine serum albuminSiliconeChromatographyPulmonary surfactantHydrolysisPolymer chemistryChemical engineeringOrganic chemistryNuclear chemistryBiochemistry

Abstract

fetched live from OpenAlex

Water-in-silicone oil emulsions were prepared using either silicone surfactants containing pendant polyethylene oxide (PEO) side chains (DC3225C) or terminal Si(OEt)3 groups. The aqueous solutions contained either the enzymes α-chymotrypsin or alkaline phosphatase (DC3225C emulsions) or the surface active protein human serum albumin (TES-PDMS emulsions). Labelled albumin was shown to reside almost exclusively at the oil/water interface in the emulsion. The activity of the enzymes was followed over time by first breaking the emulsion and then performing standard enzyme assays on the aqueous phase. The enzymes were observed to undergo denaturation, as measured by reduced enzymatic activity, as a result of the mechanical energy used to make and break the emulsion. However, the rate of enzyme denaturation in the emulsions was lower than that observed for the aqueous control which had not been exposed to silicone. These results are consistent with favorable interactions between PEO or Si(OEt)3 groups (or hydrolytic byproducts in the latter case) and the proteins that not only stabilize the interface of a water-in-oil emulsion, but also the protein, which normally would otherwise undergo efficient denaturation in the presence of silicone oil.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesInsufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Other · Consensus signal: none
Teacher disagreement score0.299
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0010.000
Scholarly communication0.0010.003
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.002

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.236
Teacher spread0.217 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2003
Admission routes2
Has abstractyes

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